Unitary solid chlorine dioxide effervescent tablet and preparation method thereof
A technology of chlorine dioxide and effervescent tablets, which is applied in botany equipment and methods, chemicals for biological control, animal repellants, etc., and can solve inconvenience, chlorine dioxide gas escape, low generation, etc. problem, to achieve the effect of improving chemical yield, accelerating dissolution rate, and enhancing bactericidal activity
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Embodiment 1
[0072] Tablets weighing 10 grams were prepared using the following formulation.
[0073] raw material name
Raw material ratio
Sodium chlorite (content ≥ 80%), kg
34
Sodium dichloroisocyanurate, kg
13
Sodium bisulfate, kg
21
20
5
Sodium alginate, kg
2.5
Sodium dodecylbenzenesulfonate, kg
0.5
Sodium carbonate, kg
1
Adipic acid, kg
3
[0074] First pour 2.5kg of sodium alginate into 60kg of water, heat up to about 80°C and stir until completely dissolved to obtain sodium alginate slurry; sieve sodium chlorite in a vibrating sieve, and take 34kg of sodium chlorite with a particle size of 40 mesh Put it into a coating machine, spray the above-mentioned prepared binder slurry for drying and coating. The drying temperature is controlled below 100°C. When the water content of the intermediate reaches belo...
Embodiment 2
[0081] Tablets weighing 1 gram were prepared using the following formulation.
[0082] raw material name
Raw material ratio
Sodium chlorite (content ≥ 80%), kg
30
Sodium dichloroisocyanurate, kg
10
Citric acid, kg
40
2
10
Sodium alginate, kg
2.5
Sodium dodecylbenzenesulfonate, kg
0.5
2
Adipic acid, kg
3
[0083] First pour 2.5kg of sodium alginate into 60kg of water, heat up to about 80°C and stir until completely dissolved to obtain sodium alginate slurry; sieve sodium chlorite in a vibrating sieve, and take 30kg of sodium chlorite with a particle size of 40 mesh Put it into a coating machine, spray the above-mentioned prepared binder slurry for drying and coating. The drying temperature is controlled below 100°C. When the water content of the intermediate reaches below 1%,...
Embodiment 3
[0090] Tablets weighing 10 grams were prepared using the following formulation.
[0091] raw material name
Raw material ratio
Sodium chlorite (content ≥ 80%), kg
12
Sodium dichloroisocyanurate, kg
6
Sodium bisulfate, kg
40
2
15
1.5
Sodium lauryl sulfate, kg
0.5
Magnesium carbonate, kg
3
Sodium chloride, kg
20
[0092] The raw material of formula is processed according to the technological process described in embodiment 1, embodiment 2, after obtaining combined raw material, on tablet machine, press the tablet with the pressure of 50KN with the punch of diameter 25mm, be pressed into the tablet of weight 10 grams, Packed in aluminum-plastic composite bag.
[0093] 10 gram tablets are dropped into 20 liters of tap water, after 15 minutes, the concentration of sampling detect...
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