Sodium lauryl polyoxyethylene (7) octyl sulfosuccinate and its preparing process
A technology of lauryl polyoxyethylene ether and octyl sulfosuccinic acid, which is applied in chemical instruments and methods, dissolution, chemical/physical processes, etc., can solve problems such as unsatisfactory product performance and complicated procedures, and reduce equipment costs. Requirements, compact process, and the effect of avoiding the influence of impurities
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[0017] In a four-necked flask equipped with a stirrer, a thermometer and a reflux condenser, the water-treated lauryl polyoxyethylene ether (7) and maleic anhydride were added sequentially at a material mass ratio (molar ratio) of 1.00:1.10, and accounted for Alkylsulfonic acid catalyst with 1% maleic anhydride mass, feed nitrogen, stir in 10-30 minutes (Example 10, 20, 30 minutes) and heat up to 140°C temperature; keep this temperature and time, holding time 150min, in the same reaction Connect the water separator to the device, and add octanol according to the mass ratio (molar ratio) of octanol:maleic anhydride=4.0:1.0 to carry out the double esterification reaction, and heat it to 200°C according to the method of the above-mentioned monoesterification reaction Temperature and timing, heat preservation and dehydration, heat preservation time is 300min, cooling, neutralization, cooling to a temperature of 20-60°C (eg 20°C, 40°C, 60°C), neutralization to a pH value of 7±0.5; n...
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