Carbon-carbon/aluminium composite material preparation method

An aluminum composite material and aluminum liquid technology, which is applied in the field of carbon-carbon/aluminum composite material preparation, can solve the problems of difficult preparation of prefabricated parts and difficult control of interface reaction

Inactive Publication Date: 2006-05-10
SHANGHAI JIAOTONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The present invention aims at the two key problems of difficulty in preparing carbon / aluminum composite material prefabricated parts and difficult control of interface reaction, based on the existing carbon-carbon composite material preparation method and carbon / aluminum composite material preparation method, a carbon-aluminum composite material preparation method is proposed. The preparation method of carbon / aluminum composite materials enables it to effectively solve the two problems of prefabricated part preparation and interface reaction control in the preparation process of carbon / aluminum composite materials, which helps to simplify the process and reduce costs, thus providing carbon / aluminum composite materials Lay the foundation for a wide range of applications

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0018] Example 1. Preparation of needle felt carbon-carbon / aluminum composite material

[0019] First, stack several layers of monolithic felts with a thickness of 0.2~2cm, then connect them into a whole by needle punching, and reach the designed fiber volume content. After carbonization at 1050℃, they are processed by chemical vapor infiltration to make needle punched felt. Carbon-carbon preforms; afterwards, a vacuum pressure impregnation process is used to compound with aluminum to form a carbon-carbon / aluminum composite material. The volume content of carbon fiber is 6%, the volume content of pyrolysis carbon is 17%, and the others are aluminum matrix.

[0020] The fabricated carbon-carbon / aluminum composite material structure of the needle-punched felt is as follows: the fibers in the plane of the preform are randomly distributed, and the arrangement ratio in each direction is roughly the same, so that the performance of the material is in-plane Isotropic. The carbon fibers i...

example 2

[0023] Example 2. Preparation of carbon felt carbon fiber laminate carbon-carbon / aluminum composite material

[0024] First, the T300 carbon fiber of the designed thickness is laid unidirectionally on a single-layer monolithic mat, and 2-20 layers of monolithic mats with carbon fibers on the surface are stacked to form a carbon fiber-carbon felt-carbon fiber sandwich structure. After needle-punching and interlinking the structure into a whole and reaching the designed initial density, the carbonization process is carried out at 1050°C, and finally the carbon fiber carbon felt laminate carbon-based framework material is formed by chemical vapor infiltration. After that, the pressure casting method is adopted, the pressure is 10MPa, the preheating temperature of the preform is 450°C, the aluminum liquid temperature is 800°C, the mold temperature is 300°C, the press pressure is 10MPa, and the pressure is maintained for 1 minute. After cooling, a carbon-carbon / aluminum composite mater...

example 3

[0027] Example 3. Preparation of unidirectional carbon fiber reinforced carbon-carbon / aluminum composite material

[0028] After laying T300 carbon fibers in a single direction in the graphite mold to the design volume content, after chemical vapor infiltration treatment, pyrolytic carbon is deposited on the surface of the fiber, and the aluminum liquid is infiltrated into the preform by the vacuum pressure impregnation process, and the carbon-carbon preform is installed Put the mold into the steel mold, and put the mold into the heating furnace after sealing. The upper furnace body and the lower furnace body are heated up respectively, the temperature of the airtight tank and the molten aluminum reaches 750℃, and the furnace is evacuated. When the vacuum degree is 1×10 -6 MPa, jack up the crucible containing the molten aluminum, immerse the closed mold mouth of the preform into the molten aluminum, and then pour nitrogen into the furnace at a pressure of 1×10 6 MPa, under the act...

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Abstract

A high thermal conductivity, low expansion carbon-carbon / aluminum composite material. Used in the field of electronic devices. The present invention is composed of carbon fiber, pyrolytic carbon, and aluminum matrix, wherein the carbon fiber is completely wrapped in the pyrolytic carbon layer, and the aluminum matrix is ​​on the outside of the pyrolytic carbon layer, wrapping the pyrolytic carbon layer and carbon fiber, and the thickness of the pyrolytic carbon layer is Between 1 and 4 μm. In the present invention, since the pyrolytic carbon and the aluminum matrix hardly have an interface reaction, the interface is very clean, and it is difficult to find the interface product Al 4 C 3 , the excellent chemical compatibility between pyrolytic carbon and aluminum matrix reduces the interfacial thermal resistance. By controlling the form of pyrolytic carbon, the pyrolytic carbon has extremely high thermal conductivity, so that the thermal conductivity of the material is effectively improved without using high thermal conductivity fibers, and a relatively low-cost thermal conductivity material is obtained. The rate exceeds 150W / mK, and the thermal expansion coefficient is 4~8×10 -6 The carbon-carbon / aluminum composite material can fully meet the demand for this material in chip thermal control and other related fields.

Description

Technical field [0001] The invention relates to a method for preparing a composite material, in particular to a method for preparing a carbon-carbon / aluminum composite material. Used in the preparation of high-performance materials. Background technique [0002] Generally, the preparation process of carbon / aluminum composite materials includes two steps: 1. Preparation of carbon fiber preforms; 2. Compounding with aluminum to form materials. At present, there are many methods for preparing carbon fiber preforms, but using a frame or mold to manually arrange fibers is still the main method for making carbon fiber preforms. Because carbon fiber itself is relatively soft, carbon fiber preforms made using current technology mainly rely on external means such as frames and molds to maintain the structure and porosity of the preforms, and therefore cannot be mechanically processed to change the shape of the preforms. In the subsequent process, the molten aluminum is hydraulically injec...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C47/02C22C47/08C22C49/06C22C101/10
Inventor 张国定孙晋良任慕苏刘臻祎
Owner SHANGHAI JIAOTONG UNIV
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