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Preparation method of high-elasticity super-hydrophobic polystyrene-based porous material

A polystyrene, super-hydrophobic technology, applied in the field of material preparation, can solve the problems of limited practical application and insignificant effect, and achieve the effect of excellent compression recovery performance, excellent mechanical performance, and wide application.

Pending Publication Date: 2022-04-19
SOUTHWEST PETROLEUM UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Such problems largely limit its practical application
Although there have been a large number of research reports on improving mechanical properties, the effect is not obvious

Method used

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  • Preparation method of high-elasticity super-hydrophobic polystyrene-based porous material
  • Preparation method of high-elasticity super-hydrophobic polystyrene-based porous material
  • Preparation method of high-elasticity super-hydrophobic polystyrene-based porous material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] A kind of highly elastic superhydrophobic polystyrene-based porous material is prepared by the following steps: (1) 2 parts by weight of sodium persulfate are dispersed in 2000 parts by weight of deionized water to obtain solution A containing sodium persulfate; (2) 2002 Parts by weight of solution A was added to 20 parts by weight of styrene, 15 parts by weight of divinylbenzene, 5 parts by weight of trimethylolpropane triacrylate, 10 parts by weight of aminopropyl terminated polydimethylsiloxane and 15 parts by weight of In the mixed solution B that part Span80 lipophilic emulsifier is formed, in 200r / min mechanical agitation emulsification 20min, obtain pre-polymerization system; (3) the pre-polymerization system that step (2) obtains is reacted 8h at 65 ℃, and the product is used first After washing with absolute ethanol, air-dry at 50° C. for 10 h to obtain a highly elastic superhydrophobic polystyrene-based porous material.

Embodiment 2

[0037] A kind of highly elastic superhydrophobic polystyrene-based porous material is prepared by the following steps: (1) 20 parts by weight of ammonium persulfate are dispersed in 1000 parts by weight of deionized water to obtain solution A containing ammonium persulfate; (2) 1020 Parts by weight of solution A was added to 40 parts by weight of styrene, 15 parts by weight of glycidyl methacrylate, 20 parts by weight of pentaerythritol triacrylate, 40 parts by weight of polyether amine and 10 parts by weight of Span80 lipophilic emulsifier. (3) react the pre-polymerization system obtained in step (2) at 40°C for 24h, wash the product with absolute ethanol first, and then drum it at 80°C After air drying for 24 hours, a highly elastic superhydrophobic polystyrene-based porous material was obtained.

Embodiment 3

[0039] A kind of highly elastic superhydrophobic polystyrene-based porous material is prepared by the following steps: (1) 20 parts by weight of cumene hydroperoxide are dispersed in 2000 parts by weight of deionized water to obtain solution A containing cumene hydroperoxide . (2) Add 2020 parts by weight of solution A to 50 parts by weight of styrene, 20 parts by weight of N,N-methylenebisacrylamide, 10 parts by weight of ethylene glycol dimethacrylate, 30 parts by weight of 1,18- In the mixed solution B of octadecanediamine and 30 parts by weight of hydroxylated lanolin lipophilic emulsifier, emulsify at 600r / min mechanical stirring for 20min to obtain a prepolymerization system; (3) the prepolymerization system obtained by step (2) After reacting at 40°C for 24 hours, the product was first washed with absolute ethanol, and then air-dried at 80°C for 24 hours to obtain a highly elastic superhydrophobic polystyrene-based porous material.

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Abstract

The invention discloses a preparation method of a high-elasticity super-hydrophobic polystyrene-based porous material, which is prepared by in-situ polymerization of styrene, a cross-linking agent A, a cross-linking agent B and an amino compound under the action of an initiator, water and a lipophilic emulsifier. The amino compound is one of 1, 12-diaminododecane, 1, 18-octadecane diamine, polyether amine, polyethyleneimine, aminopropyl terminated polydimethylsiloxane and ethidene diamine, and the amino compound is one of 1, 12-diaminododecane, 1, 18-octadecane diamine, polyether amine, polyethyleneimine, aminopropyl terminated polydimethylsiloxane and ethidene diamine; the cross-linking agent A is one of divinyl benzene, N, N-methylene bisacrylamide, glycidyl methacrylate, glycidyl acrylate and glycidyl ether; and the cross-linking agent B is one of triallyl isocyanurate, pentaerythritol triacrylate, trimethylolpropane triacrylate, ethylene glycol dimethacrylate and dipentaerythritol pentaacrylate. The porous material prepared by the preparation method disclosed by the invention has excellent hydrophobic / oleophylic performance and compression recoverable performance, and oil stain recovery and cyclic utilization of the porous material can be realized in an extrusion mode.

Description

technical field [0001] The invention relates to the technical field of material preparation, in particular to a method for preparing a highly elastic superhydrophobic polystyrene-based porous material. Background technique [0002] With the development of science and technology and the improvement of living standards, the discharge of industrial and domestic sewage is increasing, which poses a huge threat to the ecological environment and human health; Oil spill pollution has become one of the major threats to the marine environment. Methods such as gravity separation, centrifugation, ultrasonic separation, air flotation, electric field, adsorption and biological treatment are widely used in the treatment of oily wastewater. Among these methods, the application of adsorption is considered to be one of the most promising technologies due to its convenience, low cost, high efficiency, and no secondary pollution. Compared with immiscible oil / water mixtures, the separation of ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F212/08C08F212/36C08F220/32C08F222/38C08F226/06C08F222/20C08F222/14C08J9/00C08L25/08
CPCC08F212/08C08J9/00C08J2325/08C08F212/36C08F222/103C08F220/325C08F222/104C08F222/385C08F222/102C08F226/06C08F222/1006
Inventor 赵春霞黄浩然李云涛李辉向东武元鹏李嘉鑫陈曦
Owner SOUTHWEST PETROLEUM UNIV
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