Aorthite lightweight refractory material with uniform pores and preparation method thereof
A lightweight refractory material and anorthite technology, applied in the field of refractory materials, can solve the problems of inability to operate continuously, difficult to control the size of pores, unsatisfactory thermal insulation effect, etc. Evenly distributed effect
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[0025] The invention provides a method for preparing an anorthite lightweight refractory material with uniform pores, comprising the following steps:
[0026] A) ball milling 48 to 55 wt% of coal gangue and 4.5 to 6.5 wt% of pyrophyllite to obtain a ball mill slurry;
[0027] B) stirring and mixing the ball mill material, 10-14.5wt% refractory clay and 9.5-15.5wt% calcium carbonate to obtain the main ingredient mixture;
[0028] C) mixing the main material mixture, 5-10wt% high alumina cement and 6-20wt% additives (additional) to obtain a castable;
[0029] Al in the high alumina cement 2 o 3 Content > 67wt%;
[0030] D) Casting the castable into a mold, followed by drying and roasting after demoulding to obtain an anorthite lightweight refractory material.
[0031] In the present invention, the coal gangue can increase the aluminum content during the roasting process, further helping to reduce the thermal conductivity. The mass fraction of the gangue is preferably 48-55w...
Embodiment 1
[0054] Add refractory powder (54wt% coal gangue and 7wt% pyrophyllite) into a ball mill for ball milling for 6 hours until the mesh size reaches 2000 mesh.
[0055] The slurry completed by ball milling is discharged and placed in the storage tank for standby.
[0056] Stir once, extract the ball mill slurry from the stock tank and stir simultaneously with 15wt% refractory clay and 14wt% calcium carbonate for 12min, and control the temperature of the slurry below 40°C;
[0057] Secondary stirring: add 10wt% high alumina cement and 8wt% coagulant (additional) and other auxiliary materials at the same time and stir for 10 minutes. After the stirring is completed, add 6wt% cement foaming agent (additional) and stir for 30s, let it fully stir to make the bubbles more uniform .
[0058] Quantitative pouring: 32 molds are poured at one time, the pouring time is 12 minutes, and the indoor temperature is controlled at 25°C.
[0059] Static maintenance: The solidification time of the ...
Embodiment 2
[0066] Add refractory powder (55wt% coal gangue and 7wt% pyrophyllite) into a ball mill for ball milling for 6 hours until the mesh size reaches 2000 mesh.
[0067] The slurry completed by ball milling is discharged and placed in the storage tank for standby.
[0068] Stir once, extract the ball mill slurry from the stock tank and stir simultaneously with 15wt% refractory clay and 14wt% calcium carbonate for 12min, and control the temperature of the slurry below 40°C;
[0069] Secondary stirring: add 9wt% high-alumina cement and 8wt% coagulant (additional) and other auxiliary materials at the same time and stir for 10 minutes. After the stirring is completed, add 6wt% cement foaming agent (additional) 80L and stir for 25s, let it fully stir to make the bubbles more uniform.
[0070] Quantitative pouring: 28 molds are poured at one time, the pouring time is 8 minutes, and the indoor temperature is controlled at 25°C.
[0071] Static maintenance: The solidification time of the...
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