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Atomizing agent containing alkylated glycerol as well as preparation method and application of atomizing agent

A technology of alkylated glycerin and atomizing agent, applied in the application and preparation of tobacco, tobacco, etc., can solve the problems of production difficulties, irritation, troublesome operation, etc., to improve the quality of suction, improve the dryness of the throat, and the formula is simple effective effect

Active Publication Date: 2022-01-04
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In this application, there are the following problems: 1. It is necessary to pretreat the tobacco raw material in order to increase the adsorption load of the tobacco raw material to the atomizer, and the operation is troublesome
2. Glycerin has a certain sweetness. When a large amount of glycerin is used as an atomizer, consumers often experience uncomfortable symptoms such as throat dryness, irritation and sweetness when smoking heated cigarettes.
3. Some consumers are very uncomfortable with the taste of propylene glycol, and are eager to find a substitute for it to be compounded with glycerin
However, moisture is ubiquitous in the natural environment. Therefore, on the one hand, higher requirements are placed on the processing and production environment of heated cigarettes, which need to be carried out in a lower humidity environment to absorb as little moisture as possible; on the other hand , which brings difficulties to production. The tobacco material itself is soft with atomizing agents such as glycerin and propylene glycol. Tobacco materials and cigarettes continuously absorb moisture, which makes it difficult to control the moisture content of heated cigarettes produced by different seasons, different climate conditions, different batches, different teams, and different machines, resulting in quality fluctuations; on the other hand, Higher requirements are put forward for storage and transportation. The storage and transportation of tobacco materials and cigarette sticks of heated cigarettes need to reduce the exposure time in the environment and require a lower humidity environment; on the other hand, the shelf life of heated cigarettes is shortened. , Tobacco materials and cigarettes absorb moisture continuously, causing its moisture to rise continuously, and it is easy to deteriorate, which shortens the shelf life of heated cigarettes; the last aspect affects consumers' consumption experience. There is a difference in the sensory quality between the last cigarette and the last smoked cigarette

Method used

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  • Atomizing agent containing alkylated glycerol as well as preparation method and application of atomizing agent

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] An aerosol containing alkylated glycerin, prepared by the following steps:

[0034] According to parts by mass, 10 parts of glycerin, 20 parts of glycerol ether, 5 parts of ethyl pyruvate, 0.2 parts of mannitol monooleate, and 0.2 parts of polyethylene glycol 600 monooleate were prepared.

[0035] S1. Add mannitol monooleate to ethyl pyruvate at a speed of 800r / min, mix well and heat to 80°C. Then slowly add glycerin into the mixing system at a speed of 400r / min. After the addition of glycerin, first magnetically stir at 800r / min for 3min, and then sonicate for 8min at a frequency of resting for 3s after working for 3s, to obtain coating body 1.

[0036] S2. At a speed of 400r / min, add the coating body 1 to glycerol ether, and add polyethylene glycol 600 monooleate. After the addition, first stir magnetically at a speed of 800r / min for 3min, and then After working for 3s, rest for 3s and sonicate for 8min at a frequency to obtain an aerosol.

[0037] Spray the atomizin...

Embodiment 2

[0039] This example is basically the same as Example 1, except that it also includes 5 parts of carboxymethyl chitosan and 0.3 part of 40 U / ml pyruvate decarboxylase enzyme solution.

[0040] In step S2, at a rotational speed of 100 r / min, the glycerol ether, carboxymethyl chitosan and pyruvate decarboxylase are uniformly mixed to obtain a mixture.

[0041] Then at a rotating speed of 400r / min, add the coating body 1 to the mixture, and add polyethylene glycol 600 monooleate. After 3 s, rest 3 s and sonicate for 8 min to obtain an aerosol.

Embodiment 3

[0043] This example is basically the same as Example 1, except that it also includes 5 parts of carboxymethyl chitosan and 0.3 part of 40 U / ml pyruvate decarboxylase enzyme solution.

[0044] In step S2, at a rotational speed of 400r / min, the coating body 1 was added to glycerol ether, and polyethylene glycol 600 monooleate was added. After the addition was completed, magnetic stirring was first performed at a rotational speed of 800r / min for 3 minutes. Then, after working for 3s, the frequency of resting for 3s was ultrasonicated for 8min to obtain coating body 2 .

[0045] Under the rotating speed of 100r / min, the carboxymethyl chitosan and the pyruvate decarboxylase are evenly mixed to obtain the immobilized enzyme.

[0046] At a rotational speed of 100 r / min, the coated body 2 and the immobilized enzyme were evenly mixed to obtain an aerosol.

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PUM

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Abstract

The invention relates to the technical field of heating non-combustion cigarettes, in particular to an atomizing agent containing alkylated glycerol and a preparation method and an application thereof. The atomizing agent comprises glycerol, glyceryl ether and ethyl pyruvate. The preparation method comprises the following steps: coating glycerol with ethyl pyruvate to obtain a coating body 1; and coating the coating body 1 with glyceryl ether. In the application, through the structure that the glyceryl ether coats the ethyl pyruvate and the glycerol, the permeability of the atomizing agent permeating into the tobacco raw material, namely the absorptivity of the tobacco raw material to the atomizing agent, can be improved only through the interaction among the components of the atomizing agent, additional operation on the tobacco raw material is not needed, and the formula is simple and effective.

Description

technical field [0001] The invention relates to the technical field of heat-not-burn cigarettes, in particular to an atomizer containing alkylated glycerin and its preparation method and application. Background technique [0002] Heated cigarettes (HTPs), also known as heat-not-burn cigarettes or low-temperature cigarettes, are an emerging strategic development direction of the tobacco industry. It heats the tobacco substance through an external heat source, and the atomization medium, flavor components and added fragrance in the tobacco substance are heated to generate smoke similar to that of traditional cigarettes, so that consumers can get physiological satisfaction. The tobacco substances in heated cigarettes are only heated and not burned, so that the harmful components and biological toxicity of the smoke are greatly reduced, and the sidestream smoke and environmental smoke are also greatly reduced, so it is more conducive to the health of consumers. [0003] In orde...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B3/12A24B5/16A24B15/18A24F40/70A24F40/40
CPCA24B3/12A24B5/16A24B15/18A24F40/70A24F40/40
Inventor 黄龙陈义坤罗诚浩庞登红祝浩操吉学
Owner HUBEI CHINA TOBACCO IND
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