Multifunctional lubricating oil and preparation method thereof
A lubricating oil, multi-functional technology, applied in the field of lubricating oil, can solve the problems of anti-oxidation stability and anti-corrosion performance that need to be further improved
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[0023] As a preferred embodiment, the tea polyphenol chitosan nanoparticles are made according to the method of Example 2 of the Chinese Invention Patent of Application No. 20111003721.9 (this paper is inserted here as a part of the present invention by reference) Polyphenol chitosan nanoparticles.
[0024] As a preferred embodiment, the lipophilic graphene nanosheets are lipophilic graphite made according to the method of Chinese Invention Patent Example 1 of Application No. 201710118908.6 (this article is inserted herein by reference as part of the present invention) Graphene nanosheets; the sheet diameter of the lipophilic graphene nanosheets is <100nm, and the sheet diameter and thickness are <10nm.
[0025] As a preferred embodiment, the preparation method of the cyanoethoxyphosphine sulfate-based polyquaternary ammonium salt comprises the following steps: bis(diisopropylamino)(2-cyanoethoxy)phosphine, bis (Chloromethyl)sulfate is added to the organic solvent, refluxed a...
Embodiment 1
[0038]A multifunctional lubricating oil is characterized in that it is prepared from the following components in parts by weight: 1 part of cyanoethoxyphosphine sulfate-based polyquaternium salt, 6-(dibutylamino )-1,3,5-triazole-2,4-dithiol 0.3 parts, lipophilic graphene nanosheets 0.5 parts, tea polyphenol chitosan nanoparticles 0.3 parts, dispersant 0.3 parts, N,N- 0.4 parts of bis(2-hydroxyethyl)-2-aminoethanesulfonic acid, 0.1 parts of thermoplastic elastomer TPEE, and 60 parts of base oil.
[0039] The base oil is 60N base oil; the thermoplastic elastomer TPEE is selected from the thermoplastic elastomer TPEE whose brand is EM550; the dispersant is vinyl bis stearamide.
[0040] The preparation method of described cyanoethoxyphosphine sulfate-based polyquaternary ammonium salt comprises the steps of: combining two (diisopropylamino) (2-cyanoethoxy) phosphine, two (chloromethyl) sulfate Add it into an organic solvent, reflux and stir at 30°C for 4 hours, then remove the s...
Embodiment 2
[0043] A multifunctional lubricating oil is characterized in that it is prepared from the following components in parts by weight: 1.5 parts of cyanoethoxyphosphine sulfate-based polyquaternium salt, 6-(dibutylamino )-1,3,5-triazole-2,4-dithiol 0.4 parts, lipophilic graphene nanosheets 0.7 parts, tea polyphenol chitosan nanoparticles 0.4 parts, dispersant 0.35 parts, N,N- 0.45 parts of bis(2-hydroxyethyl)-2-aminoethanesulfonic acid, 0.12 parts of thermoplastic elastomer TPEE, and 63 parts of base oil.
[0044] The base oil is 60N base oil; the thermoplastic elastomer TPEE is selected from the thermoplastic elastomer TPEE whose brand is EM630; the dispersant is monoglyceride stearate.
[0045] The preparation method of described cyanoethoxyphosphine sulfate-based polyquaternary ammonium salt comprises the steps of: combining two (diisopropylamino) (2-cyanoethoxy) phosphine, two (chloromethyl) sulfate Add it into an organic solvent, reflux and stir at 35°C for 4.5 hours, then r...
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