Organic compound and organic light-emitting device using same
A technology of organic light-emitting devices and organic compounds, which is applied in the fields of OLED devices and soluble organic compounds, can solve the problems of lack of materials and achieve the effects of easy-to-obtain raw materials, reduce vibration energy loss, and high-efficiency luminous performance
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Embodiment 1
[0047] Embodiment 1: the synthesis of compound 2-6
[0048] 1. Synthesis of intermediate 2-6-2
[0049]
[0050] Add intermediate phenothiazine borate (19.97 g, 61.4 mmol), 2-6-1 (30.05 g, 61.4 mmol), tetrakis (triphenylphosphine) palladium (5 mole %) in a 500 ml reaction flask ), potassium carbonate (17.0 g, 122.8 mmol), 1,4-dioxane (200 ml) and water (50 ml). The temperature of the reaction system was raised to 80° C., and the reaction was carried out under nitrogen protection for 12 hours. After the reaction was completed, the reaction solution was cooled to room temperature and extracted with o-dichlorobenzene and water. The organic layer was dried over anhydrous magnesium sulfate, concentrated, and recrystallized to obtain the crude product through a silica gel column to obtain intermediate 2-6-2 (26.12 g, yield 70%). LC-MS: M / Z 607.21(M+H) + .
[0051] 2. Synthesis of compound 2-6
[0052]
[0053] Add intermediate 2-6-2 (12.16 g, 20 mmol), 2-bromo-3-phenylqu...
Embodiment 2
[0054] Embodiment 2: the synthesis of compound 3-2
[0055] Compound 3-2 was synthesized with reference to the method of Example 1 to obtain compound 3-2 (11.22 g, yield 78%). LC-MS: M / Z838.29(M+H) + .
Embodiment 3
[0056] Embodiment 3: the synthesis of compound 3-8
[0057] Compound 2-6 was synthesized with reference to the method of Example 1 to obtain compound 3-8 (14.79 g, yield 87%). LC-MS: M / Z914.32(M+H) + .
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