Self-cleaning amphiphobic coating for degrading NO and preparation method of self-cleaning amphiphobic coating
A kind of sparse coating and self-cleaning technology, which is applied in coatings, separation methods, chemical instruments and methods, etc., can solve the problems of reducing the durability of super-amphiphobic coatings, losing super-amphiphobic properties, and being easy to damage, and achieving improved UV stability, excellent photocatalytic activity and adsorption effect, improved anchoring effect
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Embodiment 1
[0039] A method for preparing a self-cleaning amphobic coating for degrading NO, the specific steps are as follows:
[0040] Step 1: In parts by weight, 7 parts of P25 nano-titanium dioxide were added to 70 parts of 10mol / L sodium hydroxide solution, and stirred for 2 hours to obtain a suspension;
[0041] Step 2: Add the suspension into a hydrothermal reaction kettle, and conduct a hydrothermal reaction at 150°C for 48 hours to obtain a hydrothermal product;
[0042] Step 3: Wash the hydrothermal product 5-6 times with dilute hydrochloric acid, adjust the pH to 1-2, and stir for 24 hours;
[0043]Step 4: filter the precipitate, wash with deionized water until neutral, add absolute ethanol to disperse for 24 hours, and obtain a suspension;
[0044] Step 5: Suction filter the suspension in step 4, and dry at 110°C to constant weight to obtain titanium dioxide nanotubes;
[0045] Step 6: Disperse 0.1 part of epoxy resin (E44) in 18 parts of absolute ethanol, stir until dissolv...
Embodiment 2
[0051] A method for preparing a self-cleaning amphobic coating for degrading NO, the specific steps are as follows:
[0052] Step 1: In parts by weight, 10 parts of P25 nano-titanium dioxide were added to 70 parts of 10mol / L sodium hydroxide solution, and stirred for 2 hours to obtain a suspension;
[0053] Step 2: Add the suspension into a hydrothermal reaction kettle, and conduct a hydrothermal reaction at 150°C for 48 hours;
[0054] Step 3: Wash the hydrothermal product 5-6 times with dilute hydrochloric acid, adjust the pH to 1-2, and stir for 24 hours;
[0055] Step 4: Filter the precipitate generated in step 3, wash with deionized water until neutral, add absolute ethanol to disperse for 24 hours, and obtain a suspension;
[0056] Step 5: Suction filter the suspension prepared in Step 4, and dry at 110°C to constant weight to obtain titanium dioxide nanotubes;
[0057] Step 6: Disperse 0.4 parts of epoxy resin (E44) in 18 parts of absolute ethanol, stir until dissolve...
Embodiment 3
[0063] A method for preparing a self-cleaning amphobic coating for degrading NO, the specific steps are as follows:
[0064] Step 1: In parts by weight, 12 parts of P25 nano-titanium dioxide were added to 70 parts of 10mol / L sodium hydroxide solution, and stirred for 2 hours to obtain a suspension;
[0065] Step 2: Add the suspension into a hydrothermal reaction kettle, and conduct a hydrothermal reaction at 150°C for 48 hours;
[0066] Step 3: Wash the hydrothermal product 5-6 times with dilute hydrochloric acid, adjust the pH to 1-2, and stir for 24 hours;
[0067] Step 4: Filter the precipitate generated in step 3, wash with deionized water until neutral, add absolute ethanol to disperse for 24 hours, and obtain a suspension;
[0068] Step 5: Suction filter the suspension in step 4, and dry at 110°C to constant weight to obtain titanium dioxide nanotubes;
[0069] Step 6: Disperse 0.7 parts of epoxy resin (E44) in 18 parts of absolute ethanol, stir until dissolved, add 0....
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