Germanium-arsenic-selenium-tellurium (GeAsSeTe) powder for semiconductor memory, target material and preparation method of GeAsSeTe powder
A memory and semiconductor technology, applied in chemical instruments and methods, selenium/tellurium compounds, binary selenium/tellurium compounds, etc., can solve the problem of volatile, unsuitable for large-scale industrial production of germanium, arsenic, selenium and tellurium compounds, and equipment dependence Large and other problems, to achieve the effect of uniform composition, high density and low oxygen content
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Embodiment 1
[0035] The preparation method of the GeAsSeTe powder for the semiconductor memory of the present invention comprises the following steps:
[0036] (1) Mix Se block and As block, Ge block and Te block, Ge block and Se block respectively and put them in a quartz boat and send them into the tube furnace. Nitrogen gas is first introduced into the furnace at a rate of 10 L / min and kept Exclude the air for 30 to 40 minutes. After the quartz boat is put in and continue to ventilate for 20 to 30 minutes, introduce a mixed protective atmosphere with a volume ratio of nitrogen and hydrogen of 7:3 and heat up at 5°C / min and keep it warm to obtain AsSe alloys. , GeTe alloy and GeSe alloy; the Se block and the As block are mixed according to the atomic ratio of Se and As 1:1; the Ge block and the Te block are mixed according to the atomic ratio of Ge and Te 1:1; the Ge The block and the Se block are mixed according to the atomic ratio of Ge and Se at 1:1; the heating and heat preservation ...
Embodiment 2
[0043] The preparation method of the GeAsSeTe powder for the semiconductor memory of the present invention comprises the following steps:
[0044] (1) Mix Se block and As block, Ge block and Te block, Ge block and Se block respectively and put them in a quartz boat and send them into the tube furnace. Nitrogen gas is first introduced into the furnace at a rate of 10 L / min and kept Exclude the air for 30-40 minutes. After the quartz boat is put in and continue to ventilate for 20-30 minutes, introduce a mixed protective atmosphere with a volume ratio of nitrogen and hydrogen of 7:4 and heat up at 10°C / min and keep it warm to obtain AsSe alloys respectively. , GeTe alloy and GeSe alloy; the Se block and the As block are mixed according to the atomic ratio of Se and As 1:1; the Ge block and the Te block are mixed according to the atomic ratio of Ge and Te 1:1; the Ge The block and the Se block are mixed according to the atomic ratio of Ge and Se at 1:1; the heating and heat prese...
Embodiment 3
[0050] The preparation method of the GeAsSeTe powder for the semiconductor memory of the present invention comprises the following steps:
[0051] (1) Mix Se block and As block, Ge block and Te block, Ge block and Se block respectively and put them in a quartz boat and send them into the tube furnace. Nitrogen gas is first introduced into the furnace at a rate of 10 L / min and kept Exclude the air for 30 to 40 minutes. After the quartz boat is put in and continue to ventilate for 20 to 30 minutes, introduce a mixed protective atmosphere with a volume ratio of nitrogen and hydrogen of 7:3 and heat up at 5°C / min and keep it warm to obtain AsSe alloys. , GeTe alloy and GeSe alloy; the Se block and the As block are mixed according to the atomic ratio of Se and As 1:1; the Ge block and the Te block are mixed according to the atomic ratio of Ge and Te 1:1; the Ge The block and the Se block are mixed according to the atomic ratio of Ge and Se at 1:1; the heating and heat preservation ...
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