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Production process for extracting diosgenin

A technology for the production process of diosgenin, which is applied in the field of production process for extracting diosgenin, can solve the problems of long consumption time, low yield of diosgenin, and large acid consumption, so as to improve the extraction rate and purity, fully Effects of reusing resources and shortening the production cycle

Active Publication Date: 2021-04-20
河南度帮中药生物科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The traditional acid hydrolysis method is cumbersome to operate, consumes a long time, and the yield of diosgenin is low
And because medicinal material volume is big, the consumption amount of acid is big, and the organic matter of acid degradation is many, causes sewage volume big, and environmental pollution is big, has seriously hindered the development of diosgenin industry
Use gasoline or petroleum ether to extract the hydrolyzate, and the dosage is relatively large
Moreover, 120# gasoline is a first-class explosion-proof solvent, with a high risk factor

Method used

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  • Production process for extracting diosgenin
  • Production process for extracting diosgenin
  • Production process for extracting diosgenin

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0052] Take 1kg of fresh turmeric, wash it and cut it into 0.1-1cm thin sections, wash it with water, separate the starch and turmeric residue; add the turmeric residue into 70% ethanol solution, the volume of the ethanol solution is 50L , and then ultrasonic and microwave co-processing for 300s, the microwave power was 450W at 0-60s, 400W at 60-150s, and 600W at 150-300s; The material inlet is put into the first enzymolysis stirring tank, the second enzymolysis stirring tank, the third enzymolysis stirring tank and the fourth enzymolysis stirring tank, at the same time, add 4g α-glucosidase in the first enzymolysis stirring tank , and adjust the pH to 5.3, the temperature is 55 ° C, add 4 g rhamnosidase in the second enzymolysis stirring tank, and adjust the pH to 4.1, the temperature is 35 ° C, add 6 g glucuronic acid in the third enzymolysis stirring tank Glucosidase, and adjust the pH to 6.5, the temperature is 55 ° C, add 5 g of β-glucosidase to the fourth enzymolysis sti...

Embodiment 2

[0054] Take 1 kg of fresh yam yam, wash it, cut it into small sections with a thickness of 0.1 to 1 cm, wash it with water, and separate the starch and yam residue; add the yam residue to 70% ethanol solution, and The volume of the ethanol solution is 55L, and then ultrasonic and microwave synergistic treatment is carried out for 300s. The microwave power is 480W at 0-60s, 430W at 60-150s, and 600W at 150-300s; Divide into four parts, respectively put into the first enzymolysis stirring tank, the second enzymolysis stirring tank, the third enzymolysis stirring tank and the fourth enzymolysis stirring tank through the material inlet, at the same time, in the first enzymolysis stirring tank Add 4.5g α-glucuronidase, and adjust the pH to 5.0, the temperature is 51°C, add 4.8g glucuronidase to the second enzymolysis stirring tank, and adjust the pH to 7.0, the temperature is 56°C, the third enzyme Add 5.2g rhamnosidase to the stirred tank for enzymolysis, adjust the pH to 4.5, and...

Embodiment 3

[0056] Take 1 kg of fresh pangolin, wash it, cut it into 0.1-1cm thin sections, wash it with water, separate the starch and pangolin residue; add the pangolin residue into 70% ethanol solution, the volume of the ethanol solution is 48L , and then ultrasonic and microwave co-processing for 300s, the microwave power was 460W when 0-60s, the microwave power was 420W when 60-150s, and the microwave power was 600W when 150-300s; The material inlet is put into the first enzymolysis stirring tank, the second enzymolysis stirring tank, the third enzymolysis stirring tank and the fourth enzymolysis stirring tank, at the same time, add 4g β-glucosidase in the first enzymolysis stirring tank , and adjust the pH to 4.2, the temperature is 62°C, add 5.4g rhamnosidase in the second enzymolysis stirring tank, and adjust the pH to 4.3, the temperature is 50°C, add 5.8g glucose in the third enzymolysis stirring tank aldolidase, and adjust the pH to 6.5, and the temperature is 50°C, add 5g of α...

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Abstract

The invention discloses a production process for extracting diosgenin. The production process comprises the following steps: pretreatment of raw materials: removing hairy roots of fresh dioscorea opposita plants, cleaning to remove silt, cutting into sections with a thickness of 0.1-1 cm, cleaning with water, and separating starch from dioscorea opposita residues; solvent extraction: collecting the dioscorea opposita residues, and performing solvent extraction to obtain dioscin; hydrolyzing the dioscin; and extracting, purifying and recrystallizing the hydrolysate. The production process can solve problems of waste and environmental pollution in the current acid hydrolysis and gasoline extraction, and can recycle residues, and improve extraction rate and purity of diosgenin obtained by extraction.

Description

technical field [0001] The invention relates to the technical field of extracting diosgenin, in particular to a production process for extracting diosgenin. Background technique [0002] my country is a big country of yam planting. The rhizome (turmeric) of the perennial herbaceous plant Dioscorea (D.zingiberensis) and the rhizome (D. nipponica) of the genus Dioscorea (D. nipponica) are the two species with the highest diosgenin content in my country, followed by Huangshan Medicine (D.panthaica), Chaihuangjiang (D.nipponica), Triangle leaf yam (D.deltoidea), etc. These plants are easy to grow and have a large annual output, so they have become the most important traditional Chinese medicine raw materials for the production of diosgenin in the industry. Diosgenin, known as diosgenin in industry, is the ligand of diosgenin. It is connected to the sugar group through a glycoside bond at the C-3 position. It mainly exists in the rhizome of diosgenin in the form of diosgenin, an...

Claims

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Application Information

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IPC IPC(8): C12P33/20C07J71/00
CPCY02P20/54
Inventor 李雁青付宏征
Owner 河南度帮中药生物科技股份有限公司
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