Polyamide fiber containing olive and preparation method of polyamide fiber
A nylon fiber and olive technology is applied in the field of olive-containing nylon fiber and its preparation, which can solve the problems of poor distribution, inconsistent nylon fiber performance, unsatisfactory modification effect, etc. Ineffective, tight and firm effect
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Embodiment 1
[0045] A method for preparing olive-containing nylon fibers, comprising preparation of olive extract, preparation of porous nanoparticles, preparation of porous nanoparticles containing olive extract, preparation of functional masterbatch, spinning, and post-treatment.
[0046] For the preparation of the olive extract, a predetermined number of olive leaf extracts and olive fruit extracts are mixed, ground to 150 mesh; put into 10 times the volume of absolute ethanol, stirred at 100RPM for 10min, heated to 40°C, and Ultrasonic extraction was performed for 1 h, and the solid matter was filtered out to obtain the olive extract.
[0047] For the ultrasonic extraction, the ultrasonic frequency is 20kHz, and the ultrasonic intensity is 10W / cm 2 , Ultrasonic power 350W.
[0048] The weight ratio of the olive leaf extract: olive fruit extract is 1:5.
[0049] The olive leaf extract has an oleuropein content of 33%, a hydroxytyrosol content of 16%, and a mesh size of 80 mesh.
[00...
Embodiment 2
[0078] A method for preparing olive-containing nylon fibers, comprising preparation of olive extract, preparation of porous nanoparticles, preparation of porous nanoparticles containing olive extract, preparation of functional masterbatch, spinning, and post-treatment.
[0079] For the preparation of the olive extract, a predetermined number of olive leaf extracts and olive fruit extracts were mixed, ground to 200 mesh; put into 10 times the volume of absolute ethanol, stirred at 150RPM for 15min, heated to 50°C, and carried out Ultrasonic extraction for 1.5 h, and the solid matter was filtered out to obtain the olive extract.
[0080] For the ultrasonic extraction, the ultrasonic frequency is 20kHz, and the ultrasonic intensity is 10W / cm 2 , Ultrasonic power 350W.
[0081] The weight ratio of the olive leaf extract: olive fruit extract is 1:6.
[0082] The olive leaf extract has an oleuropein content of 33%, a hydroxytyrosol content of 16%, and a mesh size of 80 mesh.
[0...
Embodiment 3
[0111] A method for preparing olive-containing nylon fiber, comprising preparation of olive extract, preparation of porous nanoparticles, preparation of porous nanoparticles containing olive extract, preparation of functional masterbatch, spinning, and post-treatment.
[0112] For the preparation of the olive extract, a predetermined number of olive leaf extracts and olive fruit extracts were mixed, ground to 200 mesh; put into 10 times the volume of absolute ethanol, stirred at 150RPM for 15min, heated to 50°C, and carried out Ultrasonic extraction for 1.5 h, and the solid matter was filtered out to obtain the olive extract.
[0113] For the ultrasonic extraction, the ultrasonic frequency is 20kHz, and the ultrasonic intensity is 10W / cm 2 , Ultrasonic power 350W.
[0114] The weight ratio of the olive leaf extract: olive fruit extract is 1:6.
[0115] The olive leaf extract has an oleuropein content of 33%, a hydroxytyrosol content of 16%, and a mesh size of 80 mesh.
[01...
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