High-pressure-bearing plugging agent for oil extraction casing pipe and processing technology thereof
The invention relates to a processing technology and a technology for a leakage plugging agent, which is applied in the field of a high pressure-bearing leakage plugging agent for oil production casings and its processing technology. Strength, weak pressure bearing capacity and other problems, to achieve the effect of strong pressure bearing capacity, enhanced sealing and less corrosion
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Embodiment 1
[0021] A high-pressure plugging agent for oil production casing, the raw material components are as follows; by weight fraction, 48 parts of MOFs-modified epoxy resin, 23 parts of solid particles, 17 parts of curing agent, 13 parts of coupling agent, curing Regulator 0.7 parts.
[0022] The solid particles are a mixture of bentonite and attapulgite, and the mass ratio of bentonite to attapulgite is 3:1.
[0023] A kind of processing technology of high pressure bearing plugging agent for oil production casing, comprises the following steps (1) MOFs-modified epoxy resin: take acrylate monomer, methacrylic acid, acrylonitrile, and its mass ratio is 75:5: 10. Dissolve in acetone solution at 8°C, add dimethyl azobisisobutyrate, raise the temperature to 48°C, react for 2.5 hours, cool, and dry in vacuum to obtain substance A; take nano-silicon nitride Dissolve in acetone solution, add substance A, stir, react at 105°C for 2 hours, and dry in vacuum to obtain substance B;
[0024] ...
Embodiment 2
[0028] A high-pressure plugging agent for oil production casing, the raw material components are as follows; by weight fraction, 51 parts of MOFs-modified epoxy resin, 25 parts of solid particles, 20 parts of curing agent, 14 parts of coupling agent, curing Regulator 1.0 parts.
[0029] The solid particles are a mixture of bentonite and attapulgite, and the mass ratio of bentonite to attapulgite is 3:1.
[0030] A kind of processing technology of high pressure bearing plugging agent for oil production casing, comprises the following steps (1) MOFs-modified epoxy resin: take acrylate monomer, methacrylic acid, acrylonitrile, and its mass ratio is 75:5: 10. Dissolve in acetone solution at a temperature of 9°C, add dimethyl azobisisobutyrate, raise the temperature to 51°C, react for 2.7 hours, cool, and dry in vacuum to obtain substance A; take nano-silicon nitride Dissolve in acetone solution, add substance A, stir, react at 112°C for 2.2 hours, and dry in vacuum to obtain substa...
Embodiment 3
[0035] A high pressure-bearing plugging agent for oil production casing, the raw material components are as follows; by weight fraction, 60 parts of MOFs-modified epoxy resin, 27 parts of solid particles, 21 parts of curing agent, 17 parts of coupling agent, curing Regulator 1.2 parts.
[0036] The solid particles are a mixture of bentonite and attapulgite, and the mass ratio of bentonite to attapulgite is 3:1.
[0037] A kind of processing technology of high pressure bearing plugging agent for oil production casing, comprises the following steps (1) MOFs-modified epoxy resin: take acrylate monomer, methacrylic acid, acrylonitrile, and its mass ratio is 75:5: 10. Dissolve in acetone solution at a temperature of 10°C, add dimethyl azobisisobutyrate, raise the temperature to 52°C, react for 3 hours, cool, and dry in vacuum to obtain substance A; take nano-silicon nitride to dissolve Add substance A to acetone solution, stir, react at 115°C for 2.5 hours, and dry in vacuum to ob...
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