A kind of dty silk containing anti-ultraviolet agent and its production process
An anti-ultraviolet agent and production process technology, applied in the manufacture of rayon, conjugated synthetic polymer rayon, melt spinning, etc. Effective anti-ultraviolet ability, high mechanical properties and stability, durable effect
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preparation example 1
[0055] Mix 1.5g ashwain, 2.2g grape seed proanthocyanidin extract, 0.6g artemisia annua extract and 3.7g chitosan cinnamaldehyde Schiff base at a temperature of 45°C, and then dry at a temperature of 75°C. get anti-ultraviolet agent;
[0056] Wherein, the chitosan cinnamaldehyde Schiff base is prepared by the following method:
[0057] Disperse 3g chitosan in 50g methanol, swell at 20°C for 12h, then add 14g cinnamaldehyde and 30g absolute ethanol, ultrasonically disperse at 40°C for 10h, filter, wash, and extract for 12h , dried under vacuum at 50°C to obtain chitosan cinnamaldehyde Schiff base.
preparation example 2
[0059] After mixing 2.5g ashwain, 1.8g grape seed proanthocyanidin extract, 0.8g artemisia annua extract and 3.5g chitosan cinnamaldehyde Schiff base at a temperature of 45°C, it was dried at a temperature of 75°C. get anti-ultraviolet agent;
[0060] Wherein, the chitosan cinnamaldehyde Schiff base is prepared by the following method:
[0061] Disperse 3g chitosan in 50g methanol, swell at 20°C for 12h, then add 14g cinnamaldehyde and 30g absolute ethanol, ultrasonically disperse at 40°C for 10h, filter, wash, and extract for 12h , dried under vacuum at 50°C to obtain chitosan cinnamaldehyde Schiff base.
preparation example 3
[0063] After mixing 2g ashwain, 2g grape seed proanthocyanidin extract, 0.7g artemisia annua extract and 3.6g chitosan cinnamaldehyde Schiff base at a temperature of 47.5 °C, it was dried at a temperature of 80 °C to obtain the antibacterial agent. UV agent;
[0064] Wherein, the chitosan cinnamaldehyde Schiff base is prepared by the following method:
[0065] Disperse 3.1g chitosan in 51g methanol, swell at 22°C for 12.5h, then add 15g cinnamaldehyde and 31g absolute ethanol, disperse by ultrasonic for 10.25h at 45°C, filter, wash, Then extract for 12.5 h, and vacuum dry at 51 °C to obtain chitosan cinnamaldehyde Schiff base.
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