Preparation method of nano zirconium oxide powder
A nano-zirconia, powder technology, applied in nanotechnology and other directions, can solve the problems of inability to mix the binder uniformly, difficult flexible molding, and decreased sintering performance.
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[0025] The invention provides a preparation method of nano zirconia powder, comprising the following steps:
[0026] (1) mixing inorganic zirconium salt, inorganic yttrium salt with water to obtain a mixed solution;
[0027] (2) adding the mixed solution obtained in the step (1) dropwise into an aqueous ammonia solution to carry out a precipitation reaction to obtain a precipitation solution;
[0028] (3) mixing the precipitation solution obtained in the step (2) with an organic solvent to obtain a precursor precipitation solution;
[0029] (4) filtering part of the precursor precipitation solution obtained in the step (3) to obtain a precursor;
[0030] (5) The precursor obtained in the step (4) is mixed with the remaining precursor precipitation solution obtained in the step (3) and then filtered to obtain a powder;
[0031] (6) Calcining the powder obtained in the step (5) to obtain nano zirconia powder.
[0032] The invention mixes inorganic zirconium salt, inorganic yt...
Embodiment 1
[0047] (1) Weigh 161.00g ZrOCl of medicine 2 ·8H 2 O and 4.55 g YCl 3 ·6H 2 O is placed in the container (inorganic zirconium salt ZrOCl 2 ·8H 2 O and inorganic yttrium salt YCl 3 ·6H 2 The ratio of the amount of O to the substance is 100:3), add deionized water to 1 liter, and stir evenly at a speed of 200r / min until a clear solution is obtained to obtain a mixed solution, wherein the concentration of zirconium ions in the mixed solution is 0.5mol / L ;
[0048] (2) Prepare an ammonia solution first, wherein the pH value is 12, and the temperature is 30°C; then the mixed solution is added dropwise to the ammonia solution at a rate of 5 mL / min, and mechanically stirred at a speed of 350 r / min to obtain a precipitate liquid; where zirconium ions in the mixed solution and NH in the ammonia solution 3 ·H 2 The ratio of the amount of O to the substance is 1:2.5;
[0049] (3) Keep the temperature of the precipitation solution at 30°C, add ethanol to it, the volume ratio of ...
Embodiment 2
[0055] (1) Weigh 85.80g Zr(NO 3 ) 4 ·5H 2 O and 3.06g Y (NO 3 ) 3 ·6H 2 O is placed in the container (inorganic zirconium salt Zr(NO 3 ) 4 ·5H 2 O and inorganic yttrium salt Y(NO 3 ) 3 ·6H 2 The ratio of the amount of O to the substance is 100:4), add deionized water, and stir evenly at a speed of 200r / min until a clear solution is obtained to obtain a mixed solution, wherein the concentration of zirconium ions in the mixed solution is 0.2mol / L;
[0056] (2) Prepare an ammonia solution first, wherein the pH value is 12, and the temperature is 50°C; then add the mixed solution dropwise to the ammonia solution at a rate of 5mL / min, and perform mechanical stirring at a speed of 400r / min to obtain a precipitate liquid; where zirconium ions in the mixed solution and NH in the ammonia solution 3 ·H 2 The ratio of the amount of O to the substance is 1:3;
[0057] (3) Keep the temperature of the precipitation solution at 50°C, add isopropanol to it, the volume ratio of th...
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