Waterproof protective garment
A technology of protective clothing and waterproof finishing, which is applied in the field of clothing, and can solve the problems of decreased flexibility, affecting the health of the wearer, and the weight of protective clothing, etc., and achieves the effects of improving stability, improving waterproof effect, and reducing surface tension
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Embodiment 1
[0042] The invention discloses a waterproof protective clothing, which comprises a one-piece garment body, the surface of the one-piece garment body is treated with a waterproof finishing agent, and the preparation method of the waterproof finishing agent is as follows:
[0043] S1. First mix dimethyl malonate, glutaraldehyde, dioctyl azelate, petroleum ether and deionized water and stir evenly, adjust the pH value to 4 with acetic acid, and stir for 3 minutes; then add cobalt naphthenate , the temperature is 45°C, the ultrasonic power is 200W, and the ultrasonic is applied for 5 minutes to obtain a mixed emulsion;
[0044] S2. Mix 2-isopropylimidazole, sodium methylsiliconate and N-methylaniline at a reaction temperature of 40°C and stir for 30 minutes to obtain a mixture;
[0045] S3. Add the mixture of hydroxy silicone oil, sodium lauryl sulfate and S2 to the mixed emulsion of S1, and add thioacetamide, adjust the temperature to 30°C, and stir for 5 minutes until uniform;
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Embodiment 2
[0050] The invention discloses a waterproof protective clothing, which comprises a one-piece garment body, the surface of the one-piece garment body is treated with a waterproof finishing agent, and the preparation method of the waterproof finishing agent is as follows:
[0051] S1. First mix dimethyl malonate, glutaraldehyde, dioctyl azelate, petroleum ether and deionized water and stir evenly, adjust the pH value to 5 with acetic acid, and stir for 5 minutes; then add cobalt naphthenate , the temperature is 50°C, the power of the ultrasonic wave is 260W, and the ultrasonic wave is applied for 10 minutes to obtain a mixed emulsion;
[0052] S2. Mix 2-isopropylimidazole, sodium methylsiliconate and N-methylaniline at a reaction temperature of 50°C and stir for 40 minutes to obtain a mixture;
[0053] S3. Add the mixture of hydroxy silicone oil, sodium lauryl sulfate and S2 to the mixed emulsion of S1, and add thioacetamide, adjust the temperature to 35°C, and stir for 8 minute...
Embodiment 3
[0058] The invention discloses a waterproof protective clothing, which comprises a one-piece garment body, the surface of the one-piece garment body is treated with a waterproof finishing agent, and the preparation method of the waterproof finishing agent is as follows:
[0059] S1. First, mix dimethyl malonate, glutaraldehyde, dioctyl azelate, petroleum ether and deionized water and stir evenly, adjust the pH value to 4.5 with acetic acid, and stir for 4 minutes; then add cobalt naphthenate , the temperature is 48°C, the ultrasonic power is 240W, and the ultrasonic is applied for 8 minutes to obtain a mixed emulsion;
[0060] S2. Mix 2-isopropylimidazole, sodium methylsiliconate and N-methylaniline at a reaction temperature of 43°C and stir for 36 minutes to obtain a mixture;
[0061] S3. Add the mixture of hydroxy silicone oil, sodium lauryl sulfate and S2 to the mixed emulsion of S1, and add thioacetamide, adjust the temperature to 32°C, and stir for 7 minutes until uniform...
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