Dealcoholized condensed double-component room-temperature vulcanized silicone rubber and preparation method thereof
A technology of room temperature vulcanization and dealcohol condensation, which is applied in the field of potting adhesives and can solve problems such as insufficient adhesion
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Synthetic example 1
[0069] Put 1 mol of N-(2-aminoethyl)-3-aminopropyltrimethoxysilane and 1 mol of 3-glycidyloxypropyltrimethoxysilane into the reaction kettle, and react under constant temperature reflux at 80°C for 2h. Then 2 mol of hexamethyldisilazane was added, the temperature was raised to 140° C. for reflux reaction for 12 hours, and small molecular products and unreacted hexamethyldisilazane were removed under reduced pressure to obtain novel silane compound 1#.
Synthetic example 2
[0071] Put 1 mol of 3-aminopropyltriethoxysilane and 1 mol of 3-glycidyloxypropyltrimethoxysilane into the reaction kettle, reflux at 70°C for 3 hours, and then add 1 mol of hexamethyldisilazol Azane was heated to 130°C for reflux reaction for 18 hours, and the small molecular product and unreacted hexamethyldisilazane were removed under reduced pressure to obtain the new silane compound 2#.
Synthetic example 3
[0073] Put 1 mol of 3-aminopropyltriethoxysilane and 0.5 mol of hexamethyldisilazane into the reaction kettle, reflux at 120°C for 24 hours, and then add 1 mol of 3-(methacryloyloxy ) Propyltrimethoxysilane, reflux reaction at constant temperature at 80°C for 2h, depressurize to remove small molecule products and unreacted hexamethyldisilazane, and obtain novel silane compound 3#.
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