Heat-resistant filter felt and its preparation method and composite filter felt made therefrom
A composite filtration and filter felt technology, applied in separation methods, filtration separation, membrane filters, etc., can solve the problems of poor heat resistance, low-strength processing, and difficulty of polyphenylene sulfide fibers, and achieve surface self-cleaning performance. Good, long service life at high temperature, excellent heat resistance
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Embodiment 1
[0033] A preparation method of a heat-resistant filter felt, the steps are as follows:
[0034] (1) prepare modified polyphenylene sulfide;
[0035] (1.1) 500 kg of polyphenylene sulfide fibers having a fineness of 1.5 denier and a length of 51 mm were immersed in 1000 kg of an aqueous solution of 0.5 wt % potassium permanganate.
[0036] (1.2) continuously feed ozone in the system of step (1.1), and fully mix, adopt the system of the high-energy electron beam irradiation step (1.1) that energy is 10Mev to carry out grafting reaction to its weight gain 25wt% simultaneously, the flow rate of ozone 800 kg / min;
[0037] (1.3) Wash and dry after taking out the reaction product to obtain modified polyphenylene sulfide;
[0038] The prepared modified polyphenylene sulfide has a glass transition temperature of 425°C, an LOI of 37%, and no molten droplets are produced during combustion. In the modified polyphenylene sulfide molecule, each sulfur atom is randomly associated with N ox...
Embodiment 2
[0045] A preparation method of a heat-resistant filter felt, the steps are as follows:
[0046] The modified polyphenylene sulfide fiber obtained in Example 1 and the polytetrafluoroethylene fiber with a denier of 2.0 denier and a length of 51 mm are blended in a mass ratio of 60:40 and then hydroentangled to obtain a heat-resistant filter. felt.
[0047] The area gram weight of the heat-resistant filter felt made is 500 grams / m 2 ; After thermo-oxidative aging for 100 hours under air conditions at a temperature of 280°C, the tensile strength retention rate is 92%.
[0048] Heat-resistant filter felt with an area weight of 80 g / m 2 The base cloth is compounded to make a composite filter felt, the base cloth is woven from yarn, and the yarn is spun from polytetrafluoroethylene fiber.
[0049] The final composite filter felt has a warp strength of 800N and a weft strength of 800N.
Embodiment 3
[0051] A preparation method of a heat-resistant filter felt, the steps are as follows:
[0052] The modified polyphenylene sulfide fiber obtained in Example 1 and the polytetrafluoroethylene fiber with a denier of 3.0 denier and a length of 51 mm were blended at a mass ratio of 70:30 and then needle punched to obtain a heat-resistant filter felt .
[0053] The area gram weight of the heat-resistant filter felt made is 600 grams / m 2 ; After thermo-oxidative aging for 100 hours under air conditions at a temperature of 280°C, the tensile strength retention rate is 94%.
[0054] Heat-resistant filter felt with an area weight of 100 g / m 2 The base cloth is compounded to make a composite filter felt, the base cloth is woven from yarn, and the yarn is spun from the modified polyphenylene sulfide fiber prepared in Example 1.
[0055] The final composite filter felt has a warp strength of 980N and a weft strength of 980N.
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