Preparation method of Ni single atom doped cobaltosic oxide nano material and product and application thereof
A technology of cobalt tetroxide and nanomaterials, applied in cobalt oxide/cobalt hydroxide, nanotechnology, analytical materials, etc., can solve problems to be further improved, and achieve improved electrical properties and catalytic properties, easy process conditions, and simple preparation methods. Effect
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Embodiment 1
[0019] A Ni single atom doped tricobalt tetroxide nanomaterial, using microwave hydrothermal reaction and subsequent heat treatment method, first using microwave hydrothermal reaction to synthesize Ni precursor solution, taking Ni precursor and placing it in Co precursor solution, continuing microwave reaction, Then the resulting product was heat-treated in a hydrogen atmosphere to obtain nickel single-atom-doped Co 3 o 4 Nanomaterials are prepared as follows:
[0020] Step 1: Take 0.5mmol of Co(NO 3 ) 2 ·6H 2 O was dissolved in 50 mL of DMF; 2 mmol of sodium citrate and 2 mmol of hexamethylenetetramine were dissolved in 50 mL of DMF, and the two were mixed and stirred evenly to obtain solution A;
[0021] Step 2: Get 0.5mmol of nickel nitrate and dissolve it in 10mL of DMF to obtain a nickel nitrate solution; get 0.2mmol of trimesic acid and dissolve it in 10mL of DMF to obtain a trimesic acid solution; dissolve the trimesic acid solution Inject the nickel nitrate soluti...
Embodiment 2
[0025] A kind of Ni single-atom doped tricobalt tetroxide nanometer material, similar to embodiment 1, is prepared according to the following steps:
[0026] Step 1: Take 2mmol of Co(NO 3 ) 2 ·6H 2 O was dissolved in 50 mL of dimethylformamide (DMF); 3 mmol of sodium citrate and 6 mmol of hexamethylenetetramine were dissolved in 50 mL of DMF, and the two were mixed and stirred evenly to obtain solution A;
[0027] Step 2: Get 0.5mmol of nickel nitrate and dissolve it in 10mL of DMF to obtain solution B nickel nitrate solution; get 0.3mmol of trimesic acid and dissolve it in 10mL of DMF to obtain solution C trimesic acid solution; Solution B was injected into solution C at a rate of 20 microliters per second, and stirred to obtain mixed solution D; the mixed solution D was transferred to a glass vessel, and reacted in a microwave reactor at 140°C for 30 minutes to obtain solution E;
[0028] Step 3: Mix 0.4mL of solution E with solution A, transfer it to a polytetrafluoroeth...
Embodiment 3
[0031] A kind of Ni single-atom doped tricobalt tetroxide nanometer material, similar to embodiment 1, is prepared according to the following steps:
[0032] Step 1: Take 2.5mmol of Co(NO 3 ) 2 ·6H 2 O was dissolved in 50mL of DMF; 1mmol of sodium citrate and 5mmol of hexamethylenetetramine were dissolved in 50mL of DMF, wherein the molar ratio of sodium citrate and hexamethylenetetramine was 1:5~5: 1. Mix and stir the two evenly to obtain solution A;
[0033]Step 2: Take 0.5 mmol of nickel nitrate and dissolve it in 10 mL of DMF to obtain solution B nickel nitrate solution; take 0.2 mmol of 2,5-dihydroxyterephthalic acid and dissolve it in 10 mL of DMF to obtain solution C; Inject solution C into solution B at a rate of 20 microliters per second, stir to obtain mixed solution D; transfer mixed solution D to a glass vessel, and react in a microwave reactor at 130°C for 30-40 minutes to obtain solution E;
[0034] Step 3: Mix 0.5mL of solution E with solution A, transfer to...
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