Melamine-epoxy glass fiber tube and preparation method thereof
A technology of epoxy glass fiber and glass fiber tube is applied in the field of melamine and epoxy composite materials and their preparation, and can solve the problems of high brittleness, adverse effects on human body and environment, and low electrical strength.
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Embodiment 1-1
[0046] At room temperature, add 20 parts of methyl etherified melamine resin, 31 parts of o-cresol novolac epoxy resin, 35 parts of phosphorus-containing epoxy resin, and 13 parts of methyl ethyl ketone into the glue mixing tank, stir for 1 hour at room temperature, add 12 parts of 4,4-diaminodiphenylsulfone, stirred for 1.5 hours, then added 12 parts of inorganic powder aluminum hydroxide, 0.02 parts of accelerator 2-methylimidazole, and continued to stir at room temperature for 0.35 hours to fully disperse and evenly, Take a sample, and use the knife method to test the molding time of the glue solution (160°C hot plate) for 336 seconds, and the glue solution is prepared.
Embodiment 1-2
[0048] At room temperature, add 20 parts of polymerized partially methylated melamine resin, 27 parts of phenolic novolac epoxy resin, 33 parts of phosphorus-containing phenolic resin, and 15 parts of N,N-dimethylformamide into the compounding tank respectively. After stirring for 1.25 hours at room temperature, add 3 parts of curing agent dicyandiamide, stir for 0.5 hours, then add 18 parts of inorganic powder hydrotalcite and 0.01 part of accelerator 2-ethyl-4-methylimidazole, and continue stirring for 0.25 hours. After fully dispersing it evenly, take a sample, and test the molding time of the glue solution (160°C hot plate) for 242 seconds with a knife method, and the glue solution is prepared.
Embodiment 1-3
[0050] At room temperature, respectively add 20 parts of butylated melamine resin, 36 parts of hydantoin epoxy resin, 37 parts of phosphorus-containing phenolic resin, 8 parts of xylene, and 9 parts of methyl ethyl ketone into the compounding tank, and stir for 1.83 hours at room temperature , add 14 parts of curing agent m-phenylenediamine, stir for 0.65 hours, then add 19 parts of inorganic powder magnesium hydroxide, 0.1 part of accelerator boron trifluoride ethylamine, continue stirring for 0.75 hours, take samples, and use the knife method to test the glue The molding time of the liquid (160°C hot plate) is 312 seconds, and the glue liquid is prepared.
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