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Surface treatment method of beryllium material for nuclear reactor and beryllium material for nuclear reactor

A technology for surface treatment and nuclear reactors, applied in the surface treatment of beryllium materials for nuclear reactors, and in the field of beryllium materials for reactors, it can solve the problems of dullness, no metallic luster, pitting or pits, etc., to meet technical requirements and reduce surface The formation probability of burning, the effect of color uniformity

Inactive Publication Date: 2020-04-17
西北稀有金属材料研究院宁夏有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, beryllium products are treated with acid liquid surface during product processing to simply eliminate internal stress and remove surface impurities. The products treated by this method have no metallic luster, are dull, or have very good brightness, but there is no formation on the surface. On the frosted surface, the formed film is dense and smooth, which affects the welding quality of the product in the later stage, and is easy to corrode the surface of the beryllium material, forming pits or pits, which cannot meet the needs of new aviation products.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Step 1. Using mechanical abrasive belt grinding, the surface finish treatment of the beryllium material for nuclear reactors is carried out to remove the tool lines processed by the machine tool and improve the surface finish.

[0026] Step 2: In an air-circulating environment, use acetone to degrease the beryllium material for nuclear reactors after the surface finish treatment.

[0027] Step 3: Prepare chemical treatment solution, mix phosphoric acid, chromium trioxide and hydrofluoric acid into glycerin, wherein, the volume ratio of phosphoric acid, hydrofluoric acid and glycerin is 400:10:30, every 30ml of glycerin Add 50g of chromium trioxide.

[0028] Step 4. Soak the beryllium material for nuclear reactor after degreasing treatment in the chemical treatment solution and stir for 1 to 3 minutes until the beryllium material for nuclear reactor floats on the surface of the chemical treatment solution, then take it out and perform surface chemical treatment solution ...

Embodiment 2

[0031] Step 1. Using mechanical abrasive belt grinding, the surface finish treatment of the beryllium material for nuclear reactors is carried out to remove the tool lines processed by the machine tool and improve the surface finish.

[0032] Step 2: In an air-circulating environment, degreasing treatment is performed on the beryllium material for nuclear reactor after the surface finish treatment by using ethanol.

[0033] Step 3: Configure chemical treatment solution, mix phosphoric acid, chromium trioxide, hydrofluoric acid and alcohol into glycerol, wherein the volume ratio of phosphoric acid, hydrofluoric acid, glycerol and alcohol is 500:15:40:15, Add 75g of chromium trioxide per 40ml of glycerol.

[0034] Step 4. Soak the beryllium material for nuclear reactor after the degreasing treatment in the chemical treatment solution and stir for 2 minutes until the beryllium material for nuclear reactor floats on the surface of the chemical treatment solution, then take it out ...

Embodiment 3

[0037] Step 1. Using mechanical abrasive belt grinding, the surface finish treatment of the beryllium material for nuclear reactors is carried out to remove the tool lines processed by the machine tool and improve the surface finish.

[0038] Step 2: In an air-circulating environment, degreasing treatment is performed on the beryllium material for nuclear reactor after the surface finish treatment by using ethanol.

[0039] Step 3: Configure chemical treatment solution, mix phosphoric acid, chromium trioxide, hydrofluoric acid and alcohol into glycerol, wherein the volume ratio of phosphoric acid, hydrofluoric acid, glycerol and alcohol is 550:12:35:5, Add 80g of chromium trioxide per 35ml of glycerol.

[0040] Step 4. Soak the beryllium material for nuclear reactor after the degreasing treatment in the chemical treatment solution and stir for 2.5 minutes until the beryllium material for nuclear reactor floats on the surface of the chemical treatment solution, then take it out...

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PUM

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Abstract

The invention discloses a surface treatment method of a beryllium material for a nuclear reactor. The surface treatment method comprises the following steps that 1, surface finishment treatment is carried out on the beryllium material for the nuclear reactor; 2, in an air circulating environment, oil removal treatment is carried out on the beryllium material for the nuclear reactor subjected to the surface finishment treatment by adopting an organic solution; 3, after weakly acidic oxygen-containing acid, chromium trioxide and hydrofluoric acid are mixed, and glycerol is added to prepare a chemical treatment liquid; and 4, after the beryllium material which is subjected to the deoiling treatment is soaked in the chemical treatment liquid, stirring is conducted until the beryllium materialfor the nuclear reactor floats on the surface of the chemical treatment liquid, the beryllium material is taken out, and the surface chemical treatment liquid cleaning is conducted. The invention further discloses the beryllium material for the nuclear reactor. The beryllium material for the nuclear reactor treated by the method is bright in surface and uniform in density, can form a frosted surface, and capable of conveniently conduct product welding.

Description

technical field [0001] The invention belongs to the technical field of beryllium material treatment, and in particular relates to a surface treatment method of beryllium material for nuclear reactors and the beryllium material for reactors. Background technique [0002] Beryllium and its alloys are widely used as new aviation products due to their excellent physical properties. Due to special environments such as the atmosphere and ocean, the surface of some beryllium products needs to be welded with other metals. Based on the current situation of enterprise aviation product research and development, in order to improve the welding quality and Surface properties, experimental research on surface chemical treatment of beryllium materials, has very practical significance. [0003] At present, beryllium products are treated with acid liquid surface during product processing to simply eliminate internal stress and remove surface impurities. The products treated by this method ha...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23G1/12
CPCC23G1/12
Inventor 杨超魏健王东新饶晓方
Owner 西北稀有金属材料研究院宁夏有限公司
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