Carrier special for front silver paste for printing fine lines step by step and preparation method
A special carrier, silver paste technology, used in cable/conductor manufacturing, semiconductor devices, conductive materials dispersed in non-conductive inorganic materials, etc. problems, to achieve the effect of improving adhesion performance, FF improvement, and solving line width problems
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preparation example Construction
[0019] The preparation process of this organic carrier is:
[0020] 1. Weigh according to the formula range of the carrier, first weigh the raw materials used for the organic carrier and place them in a stainless steel heating kettle with a high-speed shear stirring head;
[0021] 2. Seal the heating kettle, start the high-speed shear stirring head in the stainless steel heating kettle, so that the shear rate is 1000 rpm; at the same time, start the heating button, and heat the organic mixture to 60 °C at a heating rate of 5 °C / min. ℃, and keep warm for 2h;
[0022] 3. Turn off the high-speed shear stirring head and the heating button, and place the carrier for 24 hours to fully cool it;
[0023] 4. Take the cooled carrier out of the heating kettle, and pass it through a 1000-mesh stainless steel screen for negative pressure filtration;
[0024] 5. Seal the filtered carrier and store it at 25±5°C and 40-60% humidity.
[0025] The composition of organic carrier V2 includes t...
Embodiment example 1
[0034] According to the formula range of organic carrier V1, Dow STD-4 ethyl cellulose 12%, phenolic modified rosin resin 3.5%, Span 85 2.6%, butyl carbitol acetate 45%, dipropylene glycol methyl ether acetate 16%. Prepare the finished carrier V1 according to the preparation procedure of the organic carrier.
[0035] According to the formulation range of the organic carrier V2, PVB 2.4%, TDO 4.0%, diethylene glycol dibutyl ether 7.7%, propylene glycol butyl ether 2.2%, and dibutyl phthalate 4.6%, prepare the finished carrier according to the preparation process of the organic carrier V2.
[0036] According to the formula range of the special carrier, the organic carrier V1 is 60%, and the organic carrier V2 is 40%, and the special carrier 1 for the front silver paste for the ultra-fine line step-by-step printing is prepared.
[0037] Then 8.7% special carrier, 2.5% glass powder, 87.8% silver powder, and 1% silicone oil are printed, sintered and tested for terminal performanc...
Embodiment example 2
[0039] According to the formula range of organic carrier V1, Dow STD-4 ethyl cellulose 10%, phenolic modified rosin resin 3.2%, Span 85 2.0%, butyl carbitol acetate 50%, dipropylene glycol methyl ether acetate 14.8%. Prepare the finished carrier V1 according to the preparation procedure of the organic carrier.
[0040] According to the formula range of organic carrier V2, PVB 2.0%, TDO 4.0%, diethylene glycol dibutyl ether 6.5%, propylene glycol butyl ether 2.5%, and dibutyl phthalate 5.0%, prepare the finished carrier according to the preparation process of organic carrier V2.
[0041] According to the formula range of the special carrier, the organic carrier V1 is 60%, and the organic carrier V2 is 40%, and the special carrier 2 for the front silver paste for step-by-step printing of thin lines is prepared. Then 8.7% special carrier, 2.5% glass powder, 87.8% silver powder, and 1% silicone oil are printed, sintered and tested for terminal performance according to the applic...
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