Preparation method and application of ultrahigh-performance biomass-based banana peel guided activated carbon VOCs adsorbent
An ultra-high performance, biomass technology, applied in the field of adsorption materials, can solve the problems of low repeatability and complex synthesis methods, and achieve the effects of simple preparation process, good reproducibility, and preventing pore size shrinkage
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[0031] The preparation method of the ultra-high performance biomass-based banana peel-guided activated carbon VOCs adsorbent of the present invention, the preparation method comprises the following steps:
[0032] Step 1: Chop the banana peel, wash it with distilled water, put it in an oven at 100-120 ℃, and dry it overnight;
[0033] Step 2: put the dried banana peel in step 1 into a tube furnace for high-temperature carbonization;
[0034] Step 3: Grinding and pulverizing the banana peel after high-temperature carbonization to 20-100 mesh powder to prepare banana peel biochar;
[0035] Step 4: Mix banana peel biochar and KOH evenly with different alkali-carbon mass ratios. Specifically, first put KOH in deionized water, stir and dissolve, then pour banana peel biochar and stir together (the ratio of biochar to water The ratio is 1 g of biochar to 10 ml of deionized water), the stirring time is 1-3 h, and then the mixture is placed in a vacuum oven at 110-120 °C, and dried f...
Embodiment 1
[0042] Chop the banana peels, wash them and dry them in an oven at 100-120 °C, put the dried banana skins into a tube furnace for high-temperature carbonization at a temperature of 300 °C, and the carbonization time is 1-3 h, then cool naturally After reaching room temperature, the carbonized banana peel biochar was ground and mixed with KOH aqueous solution at a mass ratio of alkali to carbon ratio of 1:1, and the stirring time was 1 h. 8-12 hours to get the alkali-carbon mixture; then activate, the activation temperature is 700 ℃, the activation time is 1-3 hours, naturally cool to room temperature, take it out, wash and filter, put it in an oven at 100-120 ℃ for overnight drying Dry to get biochar VOCs adsorbent.
Embodiment 2
[0044] Chop the banana peel, wash it and put it in an oven at 100-120 ℃ for drying, put the dried banana peel into a tube furnace for high-temperature carbonization at 400 ℃, carbonization time is 1-3 h, and then cool naturally After reaching room temperature, the carbonized banana peel biochar was ground and mixed with KOH aqueous solution at a mass ratio of alkali to carbon ratio of 2:1, and the stirring time was 1 h. The alkali-carbon mixture is obtained in 8-12 hours; then activated, the activation temperature is 800 ℃, the activation time is 1-3 hours, naturally cooled to room temperature, after taking it out, wash and filter, put it in an oven at 100-120 ℃ for overnight drying Dry to get biochar VOCs adsorbent.
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