Method for preparing two-dimensional layered transition metal nanosheet gel
A transition metal, two-dimensional layered technology, applied in gel preparation, chemical instruments and methods, colloidal chemistry, etc., can solve the problems of high cost, complicated preparation process, long preparation time, etc. The effect of craftsmanship
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[0030] The invention provides a method for preparing a two-dimensional layered transition metal nanosheet gel, such as figure 1 As shown, including the following steps:
[0031] Step S1: Provide two-dimensional layered transition metal nanosheets (MXene nanosheets) with specific functional groups as a solute, and dissolve the two-dimensional layered transition metal nanosheets in a solvent to form a nano dispersion.
[0032] Specifically, the specific functional groups in the two-dimensional layered transition metal nanosheets with specific functional groups may be carboxyl groups, hydroxyl groups, ether groups, ester groups, ketone groups, carbonyl groups, acid anhydrides, epoxy functional groups, fluorine groups, and sulfonic acid groups. One or more of, amino, secondary amine, tertiary amine and aromatic functional group. The above-mentioned specific functional groups in the two-dimensional layered transition metal nanosheets with specific functional groups can improve the dispe...
Embodiment 1
[0050] Disperse the two-dimensional layered transition metal nanosheets in water, configure a 2mg / mL two-dimensional layered transition metal nanosheet aqueous solution, measure 2mL of the two-dimensional layered transition metal nanosheet aqueous solution and place it in a 5mL centrifuge tube To FeCl 2 Is a metal ion crosslinking agent, add 0.2mL of 5mg / mL FeCl to the two-dimensional layered transition metal nanosheet aqueous solution 2 Solution, the reaction temperature is room temperature, and then stand still. The obtained product is subjected to conductivity tests and electrochemical tests in different directions.
Embodiment 2
[0052] Disperse the two-dimensional layered transition metal nanosheets in water, configure a 3mg / mL two-dimensional layered transition metal nanosheet aqueous solution, measure 2mL of the two-dimensional layered transition metal nanosheet aqueous solution and place it in a 5mL centrifuge tube To FeCl 2 Is a metal ion crosslinking agent, add 0.2mL of 5mg / mL FeCl to the two-dimensional layered transition metal nanosheet aqueous solution 2 Solution, the reaction temperature is room temperature, and then stand still. The obtained product is subjected to conductivity tests and electrochemical tests in different directions.
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