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High-weather-resistant fir plate preparation method

A weather resistance, fir technology, applied in the direction of wood treatment, impregnated wood, wood impregnation, etc., can solve the problem of fir boards prone to discoloration, achieve significant economic value and social benefits, excellent wear resistance, and improve compatibility. Effect

Active Publication Date: 2020-01-24
福建省顺昌县升升木业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The invention aims at the problem that Chinese fir boards are prone to discoloration during long-term use, and provides a method for preparing fir boards with high weather resistance

Method used

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  • High-weather-resistant fir plate preparation method

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] (1) Add 2g of γ-(2,3-glycidyloxypropoxy)propyltrimethoxysilane modified nano-titanium dioxide to 100mLN, N-dimethylformamide, after ultrasonication for 30min, nitrogen gas is introduced, and the temperature is raised to 40°C, under magnetic stirring, add 0.05g ethylenediamine and 0.5g 2,4-dihydroxybenzophenone in sequence, and continue the magnetic stirring reaction for 8h; N, N-dimethylformamide was fully washed, and vacuum-dried at 40° C. for 24 hours to obtain 2,4-dihydroxybenzophenone-grafted nano-titanium dioxide;

[0023] (2) Add 20g of 2,4-dihydroxybenzophenone grafted nano-titanium dioxide, 10g of antioxidant 1010, 2g of sodium polyacrylate and 1g of polydimethylsiloxane into 1000mL of water, and mechanically stir for 60min at room temperature , ultrasonication for 60 minutes, and finally mechanical stirring for 30 minutes to obtain a mixed dispersion of 2,4-dihydroxybenzophenone grafted nano-titanium dioxide and an antioxidant;

[0024] (3) Put the fir plate s...

Embodiment 2

[0027] (1) Add 5g of γ-(2,3-glycidyloxypropoxy)propyltrimethoxysilane modified nano-titanium dioxide to 250mLN, N-dimethylformamide, after ultrasonication for 45min, feed nitrogen, and heat up to 60°C, under magnetic stirring, sequentially add 0.15g m-phenylenediamine and 0.8g 2,4-dihydroxybenzophenone, continue the magnetic stirring reaction for 6h; 250mL of N,N-dimethylformamide was fully washed, and vacuum-dried at 40°C for 24 hours to obtain 2,4-dihydroxybenzophenone-grafted nano-titanium dioxide;

[0028] (2) 40g2, 4-dihydroxybenzophenone graft nano-titanium dioxide, 15g antioxidant 2246, 5g didecyldimethylammonium chloride and 5g polyoxypropylene oxide ethylene glyceryl ether are added to 1500mL water, in At room temperature, first mechanically stir for 90 minutes, then sonicate for 90 minutes, and finally mechanically stir for 45 minutes to obtain a mixed dispersion of 2,4-dihydroxybenzophenone-grafted nano-titanium dioxide and an antioxidant;

[0029] (3) Place the fi...

Embodiment 3

[0032](1) Add 8g of γ-(2,3-glycidyloxypropoxy)propyltrimethoxysilane modified nano-titanium dioxide to 400mLN, N-dimethylformamide, after ultrasonication for 60min, feed nitrogen, and heat up to 80°C, under magnetic stirring, add 0.4g of 2-methylimidazole and 1g of 2,4-dihydroxybenzophenone in sequence, and continue the magnetic stirring reaction for 4h; N, N-dimethylformamide was fully washed, and vacuum-dried at 40° C. for 24 hours to obtain 2,4-dihydroxybenzophenone-grafted nano-titanium dioxide;

[0033] (2) Add 60g of 2,4-dihydroxybenzophenone grafted nano-titanium dioxide, 20g of antioxidant 264, 8g of sodium polyacrylate and 10g of defoamer DF7010 into 2000mL of water, mechanically stir for 120min at room temperature, and then Ultrasound for 120 minutes, and finally mechanically stirred for 60 minutes to prepare a mixed dispersion of 2,4-dihydroxybenzophenone grafted nano-titanium dioxide and antioxidant;

[0034] (3) Place the fir plate sample in an automatic vacuum p...

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Abstract

The invention discloses a high-weather-resistant fir plate preparation method, and belongs to the technical field of wood anti-aging treatment. The preparation method comprises: carrying out a reaction on 2,4-dihydroxybenzophenone and nanometer titanium dioxide to prepare 2,4-dihydroxybenzophenone grafted nanometer titanium dioxide, carrying out first modification treatment on a fir plate by usinga mixed dispersion liquid of the 2,4-dihydroxybenzophenone grafted nanometer titanium dioxide and antioxidant, and carrying out second modification treatment on the fir plate by using a polyurethaneaqueous solution. According to the invention, the prepared fir plate has advantages of excellent weather resistance, good wear resistance, good dimensional stability and remarkable economic value andsocial benefit.

Description

technical field [0001] The invention belongs to the technical field of anti-aging treatment of wood, and in particular relates to a preparation method of fir board with high weather resistance. Background technique [0002] Chinese fir is the main fast-growing timber in southern my country. It has the advantages of fast growth, straight stem shape, easy processing, and special aroma. In addition, fir is rich in resources and moderate in price, so it is widely used in furniture and interior decoration and other fields, such as flooring, luxury wooden door frames, core strips of blockboards, etc. However, during long-term use, fir boards are prone to discoloration due to the action of thermal oxygen and ultraviolet light, resulting in poor appearance. In order to improve the aging resistance of Chinese fir, Deng Shaoping (Deng Shaoping, Lin Qiaojia, Lin Zi, Ma Changcheng; Effects of accelerated aging on the properties of Chinese fir in plantation forests treated with high tem...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B27K3/52B27K3/00B27K3/08B27K3/34
CPCB27K3/007B27K3/08B27K3/34B27K3/52B27K2240/70
Inventor 毛克升
Owner 福建省顺昌县升升木业有限公司
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