Deodorant composition containing woody plant essential oil, and preparation method thereof
A technology of woody plants and deodorants, applied in botany equipment and methods, plant growth regulators, biocides, etc., can solve the problems of poisonous and harmful, strong smell of deodorants, etc., and achieve deodorization and bactericidal capabilities Strong, help respiratory organs and lung function, eliminate insomnia effect
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[0032] In actual operation, the preparation method of the N-dodecyl-4-isothiazolin-3-one comprises the following steps:
[0033]A1: Preparation of N,N'-dodecyldithiodipropionamide: Immerse a three-necked flask equipped with a mechanical stirrer, a thermometer, and a dropping funnel in an ice-salt bath, and add dithiodipropionate Methyl ester, when cooled to 0°C in an ice bath, slowly add aqueous solution of laurylamine dropwise, the reaction temperature is 0-5°C. Stir for 3-5 hours after the dropwise addition, and continue stirring for 5-8 hours after the white solid appears. After cooling down, filter with suction, wash with 15-20ml of water for 3-4 times, and dry in an oven until constant weight to obtain N,N'-dodecyldithiodipropionamide.
[0034] A2: Preparation of N-dodecyl-4-isothiazolin-3-one: The four-necked flask equipped with a mechanical stirrer, a thermometer, a dropping funnel and a condenser tube is immersed in an ice-salt bath. Connect a drying pipe and an exha...
Embodiment 1
[0049] Embodiment 1 provides a deodorant composition containing woody plant essential oil, said deodorant composition containing woody plant essential oil, comprising the following components by weight: 0.3 parts of woody plant essential oil, 0.1 part of preservative 1.1 parts of nonionic surfactants, 0.2 parts of cationic surfactants, 1.7 parts of deodorants, and 96.6 parts of water.
[0050] Wherein, the preservative is 2-methyl-4-isothiazolin-3-one, 2-methyl-5-chloro-4-isothiazolin-3-one, N-dodecyl-4- The mixture of isothiazolin-3-ones, the corresponding weight ratio is 3: 1: 1; the nonionic surfactant is the mixture of isooctyl alcohol polyoxyethylene ether and Tween 20, the corresponding weight ratio is 1:10; the cationic surfactant is soybean ethyl sulfate ethyl morpholine; the deodorant is a mixture of tea tree essential oil, tea tree essence, and cypress essence, and the corresponding weight ratio is 2:7:8 .
[0051] The preparation method of described N-dodecyl-4-is...
Embodiment 2
[0060] Embodiment 2 provides a deodorant composition containing woody plant essential oil, said deodorant composition containing woody plant essential oil, including the following components by weight: 0.2 parts of woody plant essential oil, antiseptic 0.08 parts of agent, 0.5 parts of nonionic surfactant, 0.15 parts of cationic surfactant, 1.5 parts of deodorant, and 96.6 parts of water.
[0061] Wherein, the preservative is 2-methyl-4-isothiazolin-3-one, 2-methyl-5-chloro-4-isothiazolin-3-one, N-dodecyl-4- The mixture of isothiazolin-3-ones, the corresponding weight ratio is 3: 1: 1; the nonionic surfactant is the mixture of isooctyl alcohol polyoxyethylene ether and Tween 20, the corresponding weight ratio is 1:10; the cationic surfactant is soybean ethyl sulfate ethyl morpholine; the deodorant is a mixture of tea tree essential oil, tea tree essence, and cypress essence, and the corresponding weight ratio is 2:7:8 .
[0062] This example also provides the preparation met...
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