A cesium magnesium sulfate nonlinear optical crystal and its preparation method and application
A nonlinear optics and crystal technology, applied in the direction of nonlinear optics, optics, crystal growth, etc., can solve the problems of small birefringence, large birefringence, difficult to obtain, etc., to achieve stable physical and chemical properties, good mechanical properties, The effect of moderate hardness
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0021] Example 1 Powdered Cs 2 Mg 3 (SO 4 ) 4 Compound preparation
[0022] Adopt solid phase reaction method to prepare, and its reaction equation is as follows:
[0023] Cs 2 SO 4 +3MgSO 4 =Cs 2 Mg 3 (SO 4 ) 4 .
[0024] The specific operation steps are: weigh Cs respectively 2 SO 4 1.086 g (0.003 mol), MgSO 41.083 g (0.009mol), put them into a mortar, mix and grind evenly, then put them into a corundum ceramic crucible, compact them, put them in a muffle furnace, and raise the temperature to 450 at a rate of 8 °C / hour ℃, heat preservation and sintering for 24 hours, then lower to room temperature, take it out, grind evenly, then raise the temperature to 650 ℃ at a rate of 10 ℃ / hour, sinter for 48 hours, take it out and grind it more than 2 times in the middle, and obtain the pure phase Cs 2 Mg 3 (SO 4 ) 4 compound.
[0025] After testing, the prepared Cs 2 Mg 3 (SO 4 ) 4 Nonlinear optical crystals do not contain a center of symmetry and belong to the...
Embodiment 2
[0028] Example 2 Powdered Cs 2 Mg 3 (SO 4 ) 4 Compound preparation
[0029] Adopt solid phase reaction method to prepare, and its reaction equation is as follows:
[0030] Cs 2 SO 4 +3MgSO 4 ·7H 2 O=Cs 2 Mg 3 (SO 4 ) 4 +21H 2 O↑
[0031] The specific operation steps are: weigh Cs respectively 2 SO 4 1.086 g (0.003 mol), MgSO 4 ·7H 2 O 2.218g (0.009 mol), put them into a mortar, mix and grind evenly, then pack into a corundum ceramic crucible, compact it, put it in a muffle furnace, and heat up to 500 ℃, heat preservation and sintering for 24 hours, then lowered to room temperature and taken out, ground evenly, then heated up to 630 ℃ at a rate of 55 ℃ / hour and sintered for 48 hours, took out and ground more than 2 times in the middle, and obtained pure phase Cs 2 Mg 3 (SO 4 ) 4 compound.
Embodiment 3
[0032] Example 3 Cs 2 Mg 3 (SO 4 ) 4 Crystal preparation
[0033] The Cs was prepared by melt growth 2 Mg 3 (SO 4 ) 4 Nonlinear optical crystals, which are respectively weighed Cs 2 SO 4 2.171g (0.006mol), MgSO 4 1.083g (0.009 mol), they are mixed and placed in a crystal growth furnace, kept at 860°C for more than 2 hours to melt into a melt, then measure the saturation temperature of the melt, and then cool the melt to below The saturation temperature was 5°C, and then the temperature was slowly lowered to 600°C at 0.5°C / day, and then rapidly lowered to room temperature to obtain the crystals.
[0034] The crystal of the present invention has frequency doubling effect. Figure 4 For adopting the Cs prepared by the present invention 2 Mg 3 (SO 4 ) 4 Schematic diagram of the structure of nonlinear optical devices made of crystals. At room temperature, a Q-switched Nd:YAG laser is used as the fundamental frequency light source, and the incident laser beam 2 (near...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com