A liquid non-fluorescent lubricant for drilling
A lubricant and non-fluorescence technology, which is applied in the field of drilling fluid, can solve the problems of mud cake adhesion and lubrication ability not meeting the requirements, reduce friction, high fluorescence level, etc., to ensure lubrication effect and stability, low temperature stability, Effects from a wide range of sources
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Embodiment 1
[0024] A liquid non-fluorescent lubricant for drilling
[0025] (1) Put 8 kg of sorbitan oleate and 10 kg of vegetable oleic acid into the reactor for miscibility, adjust the acidity value to 7.5, and obtain the mixture for later use;
[0026] (2) Take 150kg of palm oil and put it in the reactor, turn on the stirrer at a rate of 60r / min, take 75kg of concentrated sulfuric acid and put it in the funnel, slowly add it dropwise to the palm oil, the dropping time is 2h, and control the reaction temperature to 50 ℃, when reaching the end point of the reaction, dilute with water, wash with water, finally add 15kg of industrial sodium chloride, continue to stir for 20 minutes, after standing for stratification, the upper layer of sulfonated palm oil is separated with liquid alkali to neutralize the pH to 7.2, Obtain dehydrated sulfonated palm oil for subsequent use;
[0027] (3) Add 60kg of white oil and 6kg of dehydrated sulfonated palm oil to the mixture in turn, and finally add 8...
Embodiment 2
[0029] A liquid non-fluorescent lubricant for drilling
[0030] (1) Put 10kg of sorbitan oleate and 8kg of vegetable oleic acid into the reaction kettle for miscibility, adjust the acidity value to 7, and obtain the mixture for later use;
[0031] (2) Take 100kg of palm oil and place it in the reactor, turn on the stirrer at a rate of 60r / min, take 50kg of concentrated sulfuric acid and place it in the funnel, slowly add it dropwise to the palm oil for 2 hours, and control the reaction temperature to 50 ℃, when reaching the end point of the reaction, dilute with water, wash with water, finally add 10kg of industrial sodium chloride, continue to stir for 20 minutes, after standing for stratification, the upper layer of sulfonated palm oil is separated with liquid alkali to neutralize the pH to 7.0, Obtain dehydrated sulfonated palm oil for subsequent use;
[0032] (3) Add 56kg of white oil and 8kg of dehydrated sulfonated palm oil to the mixture in turn, and finally add 8kg of...
Embodiment 3
[0034] A liquid non-fluorescent lubricant for drilling
[0035] (1) Put 12kg of sorbitan oleate and 6kg of vegetable oleic acid into the reaction kettle for miscibility, adjust the acidity value to 8, and obtain the mixture for later use;
[0036] (2) Take 200kg of palm oil and place it in the reactor, turn on the stirrer at a rate of 60r / min, take 100kg of concentrated sulfuric acid and place it in the funnel, slowly add it dropwise to the palm oil for 2 hours, and control the reaction temperature to 50 ℃, when reaching the end point of the reaction, dilute with water, wash with water, finally add 20kg of industrial sodium chloride, continue to stir for 20 minutes, after standing for stratification, the upper layer of sulfonated palm oil is separated with liquid alkali to neutralize the pH to 7.5, Obtain dehydrated sulfonated palm oil for subsequent use;
[0037] (3) Add 56kg of white oil and 10kg of dehydrated sulfonated palm oil to the mixture in turn, and finally add 8kg ...
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