A kind of polishing type boron sulfate ester derusting liquid
A technology of sulfate ester and rust removal liquid, applied in the field of rust removal, can solve the problems of increasing processing cost, declining metal mechanical properties, affecting steel strength, etc., and achieving the effect of short rust removal time, no residue on the surface, and prevention of oxidation.
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Embodiment 1
[0024] 1. First prepare boron sulfate ester rust removal solution, the preparation steps are as follows:
[0025] (1) Put 55 parts of nonylphenol into the reaction kettle, heat to 105°C, then slowly add 2 parts of boric acid, and react for 135 minutes after the addition;
[0026] (2) After the reaction is completed, the temperature is lowered to 66° C., 3 parts of auxiliary agent glycerin is added, and the temperature is naturally lowered to normal temperature;
[0027] (3) Add 1.5 parts of S slowly under vacuum 2 o 3 , stirring while adding, after the addition, the temperature was raised to 55°C, and the reaction was carried out for 150 minutes;
[0028] (4) After the reaction is completed, the temperature is lowered to below 50°C, 2.5 parts of auxiliary agent glycerol is added, and the reaction is carried out for 110 minutes, and then the temperature is naturally lowered to below 30°C to obtain the product.
[0029] 2. Mix the prepared borosulfate derusting solution with ...
Embodiment 2
[0032] 1. First prepare boron sulfate ester rust removal solution, the preparation steps are as follows:
[0033] (1) Put 70 parts of nonylphenol polyoxyethylene ether NP-10 into the reactor, heat to 130°C, then slowly add 6 parts of boric acid, and react for 120 minutes after the addition;
[0034] (2) After the reaction is completed, cool down to 75°C, add 5 parts of auxiliary agent sorbitol, and cool down to normal temperature naturally;
[0035] (3) Slowly add 3 parts of SO under vacuum 3 , stirring while adding, after the addition, the temperature was raised to 80°C, and the reaction was carried out for 125 minutes;
[0036] (4) After the reaction is completed, cool down to below 50°C, add 5 parts of epoxy soybean oil as an auxiliary agent, react for 130 minutes, and then naturally cool down to below 30°C to obtain the product.
[0037] 2. Mix the prepared borosulfate derusting solution with alumina particles with a particle size of 1 micron and water, and stir evenly; ...
Embodiment 3
[0040] 1. First prepare boron sulfate ester rust removal solution, the preparation steps are as follows:
[0041] (1) Put 95 parts of nonylphenol polyoxyethylene ether NP-20 into the reactor, heat it to 145°C, then slowly add 13 parts of boric acid, and react for 110 minutes after the addition;
[0042] (2) After the reaction is completed, the temperature is lowered to 95° C., 11 parts of auxiliary agent propylene glycol are added, and the temperature is naturally lowered to normal temperature;
[0043] (3) Add 4.5 parts of S slowly under vacuum 2 o 3 , stirring while adding, after the addition, the temperature was raised to 95°C, and the reaction was carried out for 150 minutes;
[0044] (4) After the reaction is completed, the temperature is lowered to below 50°C, 9 parts of auxiliary agent mannitol is added, the reaction is carried out for 180 minutes, and then the temperature is naturally lowered to below 30°C to obtain the product.
[0045] 2. Mix the prepared borosulf...
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