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Method for extracting grape seed-peanut shell-chrysanthemum to prepare antibacterial, anti-inflammatory and anti-oxidization component of toothpaste

An anti-oxidant ingredient, peanut shell technology, applied in the field of toothpaste, can solve the problems of less research on chrysanthemum polysaccharides, and achieve the effects of significant antibacterial and antibacterial effects, excellent inhibitory effects, and strong antioxidant activity

Inactive Publication Date: 2019-02-22
安徽万春日化有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The research on chrysanthemum at home and abroad mainly stays in the research on the volatile oil, choline and flavonoids in chrysanthemum, and the research on chrysanthemum polysaccharide is less

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A method for extracting grape seed-peanut shell-chrysanthemum to prepare toothpaste antibacterial, anti-inflammation and antioxidant components, is characterized in that it comprises the following steps:

[0023] (1) Extraction process of grape seed proanthocyanidins by ultrasonic microwave double-assisted method:

[0024] Dried, crushed, sieved, and degreased grape seeds, added organic solvent ethanol to 10 parts of defatted grape seed powder at a solid-to-liquid ratio of 1:14, ultrasonically extracted at 40-45°C for 20 minutes, and microwave irradiated for 30 seconds, centrifuged and collected The supernatant was evaporated under reduced pressure and vacuum freeze-dried;

[0025] (2) Preparation of antibacterial extract of peanut shell luteolin:

[0026] Wash the peanut shells, dry them in an oven at 50-55°C, grind them into powder with a pulverizer, and pass through a 50-mesh sieve; add acetone aqueous solution to 10 parts of peanut shell powder at a ratio of materi...

Embodiment 2

[0034] A method for extracting grape seed-peanut shell-chrysanthemum to prepare toothpaste antibacterial, anti-inflammation and antioxidant components, is characterized in that it comprises the following steps:

[0035] (1) Extraction process of grape seed proanthocyanidins by ultrasonic microwave double-assisted method:

[0036] Dried, crushed, sieved and degreased grape seeds, added organic solvent ethanol to 20 parts of degreased grape seed powder at a solid-to-liquid ratio of 1:15, ultrasonically extracted at 40-45°C for 30min, microwave irradiated for 35s, centrifuged and collected The supernatant was evaporated under reduced pressure and vacuum freeze-dried;

[0037] (2) Preparation of antibacterial extract of peanut shell luteolin:

[0038] Wash the peanut shells, dry them in an oven at 50-55°C, grind them into powder with a pulverizer, and pass through a 50-mesh sieve; add acetone aqueous solution to 20 parts of peanut shell powder at a material-to-liquid ratio of 1:2...

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PUM

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Abstract

The invention discloses a method for extracting grape seed-peanut shell-chrysanthemum to prepare an antibacterial, anti-inflammatory and anti-oxidization component of toothpaste. The method comprisesthe following steps: drying grape seeds, crushing, sieving and degreasing; adding an organic solvent ethanol into degreased grape seed powder; carrying out ultrasonic extraction and then carrying outmicrowave radiation extraction; centrifuging and collecting supernatant; decompressing and carrying out rotary evaporation; freezing and drying in vacuum; washing peanut shells and drying; drying thepeanut shells into powder through a pulverizer and sieving; adding an acetone water solution into peanut shell powder; refluxing and extracting in a water bath; filtering and collecting filtrate; carrying out rotary evaporation and concentration; making the capacity constant until a product has a semi-extract state, and putting the product into a vacuum drying box; drying to obtain peanut shell antibacterial extract; removing flower buds of dried chrysanthemums, sieving and removing powder; adding water into the chrysanthemums; then adding cellulase and extracting; carrying out rotary evaporation and concentration on an extracting solution; carrying out alcohol precipitation with ethanol to obtain chrysanthemum polysaccharide; and uniformly mixing and compounding the chrysanthemum polysaccharide, grape seed procyanidin and the peanut shell antibacterial extract to prepare the antibacterial, anti-inflammatory and anti-oxidization component of the toothpaste.

Description

technical field [0001] The invention belongs to the technical field of toothpaste, and in particular relates to a method for preparing antibacterial, anti-inflammatory and anti-oxidative components of toothpaste by extracting grape seeds-peanut shell-chrysanthemum. Background technique [0002] Chrysanthemum is one of the top ten famous flowers in my country, which has high ornamental value, and chrysanthemum also has high medicinal value and nutritional value. The research on chrysanthemum at home and abroad mainly stays in the research on the volatile oil, choline and flavonoids in chrysanthemum, and the research on chrysanthemum polysaccharide is less. Peanut shells are rich in luteolin, which is a flavonoid compound with antibacterial, anti-inflammatory, and antioxidant effects. [0003] The present invention extracts grape seeds, peanut shells and chrysanthemums to obtain grape seed proanthocyanidins extracts, peanut shell antibacterial extracts and chrysanthemum polys...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K8/9789A61K8/73A61K8/49A61Q11/00A61P31/02A61P31/04A61P29/00A61P39/06
CPCA61K8/498A61K8/73A61K2800/805A61K2800/82A61Q11/00A61K8/9789A61P29/00A61P31/02A61P31/04A61P39/06
Inventor 刘宁
Owner 安徽万春日化有限公司
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