Preparation method of surface silicide coating for TZM (Titanium-Zirconium-Molybdenum) alloy sheet
A technology of silicide and thin plate, which is applied in the field of preparation of silicide coating on the surface of TZM alloy thin plate, can solve the problems of high brittleness of the coating, peeling off of the coating, weak coating adhesion, etc., so as to improve the joint strength and avoid a large number of The effect of dissolving and improving mechanical properties
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Embodiment 1
[0027] Example 1: First, the surface of a TZM alloy sheet with a thickness of 4 mm was polished, cleaned with alcohol and dried, and then a pure Al element layer with a thickness of 15 μm was sputtered on the molybdenum alloy by magnetron sputtering. Ball mill the alloy powder composed of Mo 52%, Nb11%, Al 4.5%, and the balance Si. The milling time is 22h and the rotation speed is 250r / min; use CO 2 Laser, cladding alloy powder on TZM alloy thin plate sputtered with pure Al element layer by synchronous powder feeding method, powder feeding speed 6g / min, argon flow 7L / min, laser power 1.2kW, scanning speed 10mm / s.
[0028] The bond strength between the substrate and the coating measured by experiments is 7.8MPa. Compared with Comparative Example 1, the bond strength between the substrate and the coating is significantly improved under the same laser process parameters. figure 1 This is the metallographic structure of the cross-section of the silicide coating on the surface of the T...
Embodiment 2
[0029] Example 2: First, the surface of a TZM alloy sheet with a thickness of 3 mm was polished, and then a pure Al element layer with a thickness of 10 μm was sputtered on the TZM alloy by magnetron sputtering. Ball mill the alloy powder with a mass percentage of 58% Mo, 8.0% Nb, 5.5% Al, and the balance Si. The milling time is 20h and the rotation speed is 300r / min; use CO 2 Laser, cladding alloy powder on TZM alloy thin plate sputtered with pure Al element layer by synchronous powder feeding method, powder feeding speed 6g / min, argon flow 7L / min, laser power 1.0kW, scanning speed 6mm / s. The bond strength between the substrate and the coating was measured to be 8.1MPa through experiments.
Embodiment 3
[0030] Example 3: First, the surface of a TZM alloy sheet with a thickness of 3 mm was polished, and then a pure Al element layer with a thickness of 10 μm was sputtered on the TZM alloy by magnetron sputtering. The alloy powder composed of Mo 63%, Nb 6.5%, Al 3.5%, and the balance Si is subjected to long-term ball milling. The milling time is 20h and the speed is 300r / min; use CO 2 Laser, cladding alloy powder on TZM alloy thin plate sputtered with pure Al element layer by synchronous powder feeding method, powder feeding speed 6g / min, argon flow 7L / min, laser power 1.2kW, scanning speed 10mm / s. The bond strength between the substrate and the coating is 7.7MPa measured by experiments.
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