Preparation method of modified cotton fiber material
A fiber material and modified cotton technology, applied in the directions of light-resistant fibers, fiber processing, plant fibers, etc., can solve the problems of poor stability, easy yellowing of fabrics, narrow absorption wavelength range, etc., and achieve high durability and simple finishing process. Effect
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[0018] The invention discloses a preparation method of a modified cotton fiber material, comprising:
[0019] (1) adding an appropriate amount of nano-zinc oxide particles to a polyethylene glycol solution with a certain mass percentage, adjusting the pH value to 6.5-7.5, ultrasonically dispersing for 1-2 hours, and standing to obtain a modified zinc oxide dispersion;
[0020] (2) Add chitosan imine solution to the above-mentioned modified zinc oxide dispersion, control the temperature condition to be 20-30°C, and ultrasonically disperse for 2-5 hours to obtain a modified zinc oxide-chitosan imine dispersion;
[0021] (3) Alkaline washing, desizing, and oxidation treatment are carried out on the cotton fiber material, placed in the finishing agent containing the above-mentioned modified zinc oxide-chitosan imine dispersion, and the cotton fiber material is treated by the "two dipping and two rolling" process Carry out modification and finishing, dry the cotton fiber material a...
Embodiment 1
[0027] (1) adding an appropriate amount of nano zinc oxide particles to a polyethylene glycol solution with a mass percentage of 3%, adjusting the pH value to 6.5, ultrasonically dispersing for 1 hour, and standing to obtain a modified zinc oxide dispersion;
[0028] (2) Add chitosan imine solution to the modified zinc oxide dispersion with a volume ratio of 2.5:1, control the temperature at 20°C, and ultrasonically disperse for 2 hours to obtain modified zinc oxide-chitosan imine Dispersions;
[0029] (3) Alkaline washing, desizing, and oxidation treatment are carried out on the cotton fiber material, placed in the finishing agent containing the above-mentioned modified zinc oxide-chitosan imine dispersion, and the cotton fiber material is treated by the "two dipping and two rolling" process Carry out modification and finishing, the cotton fiber material after padding is dried at 70°C for 5 minutes, then soaked in deionized water for 24 hours, dehydrated, and dried at 60°C fo...
Embodiment 2
[0031] (1) adding an appropriate amount of nano zinc oxide particles to a polyethylene glycol solution with a mass percentage of 5%, adjusting the pH value to 7, ultrasonically dispersing for 1.5 hours, and standing to obtain a modified zinc oxide dispersion;
[0032] (2) Add chitosan imine solution to the modified zinc oxide dispersion with a volume ratio of 3:1, control the temperature at 25°C, and ultrasonically disperse for 3.5 hours to obtain modified zinc oxide-chitosan imine Amine dispersion;
[0033] (3) Alkaline washing, desizing, and oxidation treatment are carried out on the cotton fiber material, placed in the finishing agent containing the above-mentioned modified zinc oxide-chitosan imine dispersion, and the cotton fiber material is treated by the "two dipping and two rolling" process Carry out modification and finishing. The cotton fiber material after padding is dried at 80°C for 6 minutes, soaked in deionized water for 24 hours, dehydrated, and dried at 70°C f...
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