Preparation method of composite zirconia ceramic backboard
A zirconia ceramic and zirconia technology, which is applied in the field of preparation of composite zirconia ceramic backplanes, can solve the problems of high energy consumption, low product yield, limited production capacity, etc., and achieve simple and controllable process, high-efficiency preparation, and compact structure Effect
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Embodiment 1
[0028] A method for preparing a composite zirconia ceramic back plate, comprising the following steps:
[0029] (1) Pour the composite zirconia granulation powder into the mold of the three-dimensional mobile phone backplane, and hold the pressure at 200Mpa for 30s to form the dry press. Among them, the composition of the composite zirconia granulation powder is shown in Table 1;
[0030] (2) Place the model obtained in step (1) in the air and degrease at 470°C for 2.0 hours to prepare a green body;
[0031] (3) placing the green body obtained in step (2) in air at 930° C. for 50 seconds;
[0032] (4) Place platinum electrodes on both sides of the biscuit obtained in step (3) and pass direct current, increase the voltage linearly at a rate of 60V / s until flashing occurs, keep the current at 950A and maintain it for 20s, and then cool down to room temperature The sintered body of the back plate can be obtained.
[0033] Field emission electron microscopy (SEM) was performed o...
Embodiment 2
[0035] A method for preparing a composite zirconia ceramic back plate, comprising the following steps:
[0036] (1) Pour the composite zirconia granulation powder into the mold of the three-dimensional mobile phone backplane, and hold the pressure at 220Mpa for 20s to form the dry press. Among them, the composition of the composite zirconia granulation powder is shown in Table 1;
[0037] (2) Place the model obtained in step (1) in the air and degrease at 400°C for 2.5 hours to prepare a green body;
[0038] (3) Place the biscuit obtained in step (2) in the air and bake at 1000°C for 40s;
[0039] (4) Place platinum electrodes on both sides of the biscuit obtained in step (3) and pass direct current, increase the voltage linearly at a rate of 20V / s until flashing occurs, keep the current at 1000A for 30s, and then cool down to room temperature The sintered body of the back plate can be obtained.
[0040] Field emission electron microscopy (SEM) was performed on the obtained ...
Embodiment 3
[0042] A method for preparing a composite zirconia ceramic back plate, comprising the following steps:
[0043] (1) Pour the composite zirconia granulation powder into the three-dimensional mobile phone backplane mold, and hold the pressure at 230Mpa for 40 seconds to form dry pressing. Among them, the composition of the composite zirconia granulation powder is shown in Table 1;
[0044] (2) Place the model obtained in step (1) in the air and degrease at 500°C for 3.0 hours to prepare a green body;
[0045] (3) placing the green body obtained in step (2) in air at 900° C. for 30 seconds;
[0046] (4) Place platinum electrodes on both sides of the biscuit obtained in step (3) and pass direct current, increase the voltage linearly at a rate of 100V / s until flashing occurs, then keep the current constant at 800A for 40s, and cool down to room temperature A back plate sintered body can be obtained.
[0047] Field emission electron microscopy (SEM) was performed on the obtained b...
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