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Flame-retardant single-faced velvet composite fabric and preparation method and application thereof

A composite fabric, flame retardant composite technology, applied in the field of flame retardant materials, can solve the problems of environmental protection, flame retardant, cost is not easy to take into account, flame retardant is difficult to achieve LOI, etc. The effect of good performance and low fogging value

Active Publication Date: 2018-11-09
杭州中隽科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0021] Moreover, due to the open-cell structure of conventional sponge (polyurethane soft foam), it is difficult to achieve LOI greater than 27% in flame retardancy, while maintaining excellent mechanical properties and environmental performance, and the environmental protection, flame retardancy, and cost of flame-retardant textile composites. It is not easy to balance

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Flame-retardant single-faced velvet composite fabric and preparation method and application thereof
  • Flame-retardant single-faced velvet composite fabric and preparation method and application thereof
  • Flame-retardant single-faced velvet composite fabric and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0073] Weigh 266.8 grams of isophorone diisocyanate (Bayer, Germany), 191.2 grams of phosphorus-containing polyester diol DM1304 (product of Beijing Demei Kechuang Technology Co., Ltd., molecular weight 478, hydroxyl value 233mgKOH / g, phosphorus content 19.7 % (wt, %)), 200 gram polyether polyols N210 (Nanjing Zhongshan Chemical Co., Ltd.), 33.5 gram dimethylol propionic acid (0.25 moles) (Jiangxi Tianlan Industrial Co., Ltd.) carry out polycondensation reaction, control reaction temperature At 80°C, react under stirring and heating for 2.5 hours, then add 13.4 grams of trimethylolpropane (Jilin Petrochemical Company) (0.1 mol) and 13.4 grams of butanone, and react at 80°C for 1 hour;

[0074] Add 80 grams of butanone to reduce the viscosity. After the temperature of the reaction system drops below 40°C, neutralize with 26.91 grams of triethylamine. The molar ratio of triethylamine to dimethylol propionic acid is 1:1, and the degree of neutralization is controlled. at 100%;

...

Embodiment 2

[0077] Take by weighing 218.4 grams of hexamethylene diisocyanate (Bayer Corporation of Germany), 102.1 grams of N, N-bis(2-hydroxyethyl) aminomethylene phosphonic acid diethyl ester, 300 grams of polyether polyol N220 (Nanjing Zhong Mountain Chemical Co., Ltd.), 44.7 grams (0.334 moles) of dimethylol propionic acid (Jiangxi Tianlan Industrial Co., Ltd.) for polycondensation reaction, control the reaction temperature at 80 ° C, react under stirring and heating for 2.5 hours, then add 16.1 grams (0.12 mol) trimethylolpropane (Jilin Petrochemical Company) and 16.1 gram butanone, reacted 1 hour at 82 ℃;

[0078] Add 70 grams of butanone to reduce the viscosity. After the temperature of the reaction system drops below 40°C, neutralize with 33.69 grams of triethylamine. The molar ratio of triethylamine to dimethylolpropionic acid is 1:1, and the degree of neutralization is controlled. at 100%;

[0079] Add 664.0 grams of ionized water, under the speed of 1300RPM, high-speed emulsi...

Embodiment 3

[0081] Weigh 956 grams of phosphorus-containing polyester diol DM1304 (Beijing Demei Kechuang Technology Co., Ltd. DM1304, molecular weight 478, hydroxyl value 233mgKOH / g, phosphorus content (wt, %) 19.7%), 134 grams of dimethylol propane Acid and 400 grams of polyether polyol N210 (Nanjing Zhongshan Chemical Co., Ltd.), drop 870 grams of toluene diisocyanate (Yantai Wanhua Chemical Group Co., Ltd.) to carry out polycondensation reaction, control the molar ratio NCO / OH in the material at 1.5 : 1, add 100 gram butanone, react 2.0 hours at 78 ℃;

[0082] Use 298.3 grams of methyl ethyl ketone oxime (Zhejiang Quzhou New Future Chemical Co., Ltd.) to cap the remaining NCO at the end group, and react at 70°C for 1.0 hour;

[0083] Neutralize with 101 grams of triethylamine, the molar ratio of triethylamine to dimethylolpropionic acid is 1:1, and the neutralization degree is controlled at 100%;

[0084] Add 2448.4 grams of deionized water, emulsify at a high speed at 1400RPM, emuls...

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Abstract

The invention discloses a flame-retardant single-faced velvet composite fabric, which comprises a flame-retardant surface layer and flame-retardant single-faced velvet. The fire-retardant surface layer is flame-retardant PVC artificial leather, phosphorus-containing flame-retardant polyurethane synthetic leather, or flame-retardant fabric prepared from a phosphorus-containing flame-retardant polyester polymer material, wherein the LOI is not less than 27%. The flame-retardant single-faced velvet is prepared from a phosphorus-containing flame-retardant polyester polymer material. Gram weight ofthe flame-retardant single-faced velvet is 150-450 g / m<2>, velvet height is 1-10 mm, and the LOI is not less than 27%. The composite fabric of the invention has good flame-retarding effect, comfortable and soft hand feeling, good resilience, wide application range and good dimensional stability. The composite fabric has characteristics of dry cloth, environmental protection, low smoke and low toxicity, low VOC, low atomization value, no odor, soft hand feeling, excellent flame retardant performance, high peeling strength, good resilience, comfortable hand feeling and good heat preservation. The composite fabric is applicable to seats, ceilings, door panels, safety seats, sofas, soft chairs and deck chairs for high-speed railway, bullet trains, suburban railway, coaches and cars.

Description

technical field [0001] The invention relates to the field of flame-retardant materials, in particular to a flame-retardant single-face fleece composite fabric and its preparation method and application. Background technique [0002] In recent years, traffic interior combustion accidents have occurred frequently, especially for textile composites or leather composites with upholstered fillings. Cases of mass deaths and injuries caused by fires are not uncommon. It is imminent to improve the flame retardant performance of composite fabrics in the application fields of high-speed rail, bullet train, urban railway, passenger car, car seat, ceiling, door panel, safety seat, sofa, soft chair, recliner and so on. [0003] The combustion test standard for vehicle interior materials is one of the important factors to ensure vehicle safety. All countries have clear regulations on the flammability of automotive interior fabrics. my country has proposed new standards on the flame retar...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B32B7/12B32B27/02B32B27/36B32B27/06B32B33/00B32B37/12B32B37/06B32B37/10D06M15/579
CPCD06M15/579B32B5/02B32B7/12B32B27/08B32B27/18B32B33/00B32B37/06B32B37/10B32B37/12B32B37/1284D06M2200/30B32B2307/3065B32B2037/1276B32B2262/0276B32B2605/08B32B2605/00B32B2479/00
Inventor 曾军陈忠刚胡琪朱杨莉蒋小云蒋义赏孟凡超唐俊毅刘清华匡志宏
Owner 杭州中隽科技有限公司
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