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A kind of ultra-thin facial mask paper with high water retention and high softness and its preparation method and application

A mask paper and softening technology, applied in the field of high water retention, high softness and ultra-thin mask paper and its preparation, can solve the problems of limited ability to absorb active ingredients, not obvious improvement of wet strength, lack of data support, etc., and achieve excellent water retention and The effect of adsorption, easy operation and simplified process

Active Publication Date: 2019-10-18
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Chinese patent application No. 2012101905524 has announced "manufacturing method of mask paper and beauty skin care paper mask and mask". The method is based on wood fiber, bamboo fiber and grass fiber, adding nutrient solution and wet strength agent to improve wet strength Water retention, make the skin moist and transparent, and glow with natural brilliance, but the increase in wet strength is not obvious, and there is a lack of direct data support
Chinese patent application No. 2016210258688 discloses "a mask paper and its mask", which specifically relates to a theoretical design of the contour structure of a mask paper. Even though the scheme is theoretically feasible, it is difficult to produce it in an industrialized manner
Chinese patent application No. 2015104391348 announced "a production process for high water retention and tensile facial mask paper". The specific method is to use pulp as a thin material and synthetic long fibers or short fibers as a thin layer of reticular fibers. The two are compounded, and then The facial mask paper is obtained by spunlace and drying. Although the facial mask paper has water retention and stretching ability, because the pulp paper is used as the thin material and the synthetic long fiber or short fiber is used as the network fiber thin layer, the specific surface area is relatively low and the absorption is effective. Component capacity is limited

Method used

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  • A kind of ultra-thin facial mask paper with high water retention and high softness and its preparation method and application
  • A kind of ultra-thin facial mask paper with high water retention and high softness and its preparation method and application
  • A kind of ultra-thin facial mask paper with high water retention and high softness and its preparation method and application

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] A high water retention, high softness and ultra-thin facial mask paper, the preparation method of which is as follows:

[0036] (1) Soak 100g of softwood pulp in a mixed solution (1mol / L buffer) of citric acid and sodium hydroxide with a molar ratio of 1:0.1 for 6h, and then wash with deionized water at a stirring speed of 200r / min To neutrality, add deionized water to obtain a pulp with a mass fraction of 5%.

[0037] (2) get the mass fraction that obtains in step (1) and be 20L of pulp of 5%, pulverize with ultrafine particle pulverizer (Japan Zengxing Industrial Co., Ltd., model: MKCA6-2J), and the rotating speed is 200r / min, and the gap is 20 μm , cyclically pulverized 10 times to obtain cellulose nanofibrils.

[0038] (3) Ester-based quaternary ammonium salt softening agent is added to the cellulose nanofibrils obtained in step (2), and the speed of rotation is 2000r / min, and it is uniformly decomposed, and then the decomposed slurry is paper-made to obtain a faci...

Embodiment 2

[0040] A high water retention, high softness and ultra-thin facial mask paper, the preparation method of which is as follows:

[0041] (1) Soak 100g of softwood pulp in a mixed solution (1mol / L buffer) of citric acid and sodium hydroxide molar ratio of 1:1 for 12h, the stirring speed is 1000r / min, and then wash with deionized water To neutrality, deionized water was added to obtain a pulp with a consistency of 2%.

[0042] (2) Get 20L of pulp with a mass fraction of 2% obtained in step (1), pulverize it with an ultrafine pulverizer, the rotating speed is 500r / min, the gap is 0 μm, and circulate pulverized 15 times to obtain cellulose nanofibrils.

[0043] (3) Ester-based quaternary ammonium salt softener is added to the cellulose nanofibrils obtained in step (2), and the speed of rotation is 4000r / min, and it is uniformly decomposed, and then the decomposed slurry is paper-made to obtain a facial mask Paper, wherein the softening agent accounts for 2% of the mass of cellulose...

Embodiment 3

[0045] A high water retention, high softness and ultra-thin facial mask paper, the preparation method of which is as follows:

[0046] (1) Soak 100g softwood pulp in a mixed solution (1mol / L buffer) of citric acid and sodium hydroxide molar ratio of 1:10 for 1h, stirring speed 2000r / min, then wash with deionized water until Neutral, plus deionized water to obtain a consistency of 4% pulp.

[0047] (2) Get 20L of pulp with a mass fraction of 4% obtained in step (1), pulverize it with an ultrafine pulverizer, the rotating speed is 1000r / min, the gap is -20 μm, and the circulation pulverizes 20 times to obtain cellulose nanofibrils.

[0048] (3) Ester-based quaternary ammonium salt softening agent is added to the cellulose nanofibrils obtained in step (2), and the speed of rotation is 8000r / min, and it is uniformly decomposed, and then the decomposed slurry is paper-made to obtain a facial mask Paper, wherein the softening agent accounts for 3% of the mass of cellulose nanofibri...

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Abstract

The invention discloses ultrathin facial-mask paper with high water retention and high softness, a preparation method and application thereof. The method comprises the following steps of: (1) placingplant-fiber paper pulp into buffering solution to soak for 1-48 hours, then washing to be neutral, then adding water to dilute, and obtaining plant-fiber paper pulp I, wherein the buffering solution is aqueous mixed solution of citric acid and sodium hydroxide, and the mass concentration of the plant-fiber paper pulp I is 0.1%-5%; (2) adopting an ultrafine-particle crusher to crush the plant-fiberpaper pulp I obtained in the step (I), and obtaining cellulose nanofibril; (3) adding a softening agent into the cellulose nanofibril obtained in the step (2), carrying out paper making and drying after uniformly stirring and mixing, and obtaining the ultrathin facial-mask paper with high water retention and high softness. The ultrathin facial-mask paper disclosed by the invention has the beneficial effects that base materials with biodegradability are adopted, so that no influence is caused on the environment, and the prepared facial-mask paper not only has good air permeability and softness, but also has excellent water retention and adsorbability.

Description

technical field [0001] The invention belongs to the field of cosmetics, and in particular relates to a super-thin facial mask paper with high water retention and high softness, its preparation method and application. Background technique [0002] With the improvement of people's living standards, the requirements for beauty are getting higher and higher, and women are more interested in beauty care products. Because of its high nutritional content and remarkable skin care effect, facial masks have become the most important part of skin care products, which has given birth to people's deeper research on facial masks. [0003] Chinese patent application No. 2012101905524 has announced "manufacturing method of mask paper and beauty skin care paper mask and mask". The method is based on wood fiber, bamboo fiber and grass fiber, adding nutrient solution and wet strength agent to improve wet strength It retains water, makes the skin moist and transparent, and glows with natural b...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D21H27/00D21B1/34D21F11/00A61K8/98A61K8/9794A61K8/9789A61K8/9728A61K8/73A61K8/44A61K8/02A61Q19/00A61Q19/02
Inventor 王斌葛洲李金鹏陈克复
Owner SOUTH CHINA UNIV OF TECH
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