Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Method for measuring impurity elements aluminum, phosphor and titanium in nickel concentrate ores

A technology of impurity elements and concentrates, applied in the field of determination of impurity elements aluminum, titanium, and phosphorus in nickel concentrates, can solve the problems of difficult analysis of large quantities of samples, expensive instruments, and limited number of digested samples, etc., to achieve the analysis cycle. Short, strong anti-matrix interference, good accuracy

Inactive Publication Date: 2018-09-07
BAIYIN NONFERROUS GROUP
View PDF9 Cites 12 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Impurity elements such as aluminum, calcium, cobalt, chromium, copper, manganese, magnesium, nickel, lead, zinc, etc. in nickel concentrate have been digested by microwave samples and determined by inductively coupled plasma atomic emission spectrometry. The number of digested samples is limited, the cost of the instrument is too expensive, and the hidden dangers of high pressure (possible overpressure) make it difficult to analyze industrial large-scale samples

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for measuring impurity elements aluminum, phosphor and titanium in nickel concentrate ores
  • Method for measuring impurity elements aluminum, phosphor and titanium in nickel concentrate ores
  • Method for measuring impurity elements aluminum, phosphor and titanium in nickel concentrate ores

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0023] The present invention will be described in detail below in combination with specific embodiments.

[0024] 1, the present invention uses reagent and instrument measurement parameter in assay process to have:

[0025] (1) Reagent preparation:

[0026] 1.1. Hydrochloric acid: ρ1.19g / mL, superior grade.

[0027] 1.2. Nitric acid: ρ1.42g / mL, superior grade.

[0028] 1.3. Hydrofluoric acid: ρ1.16g / mL.

[0029] 1.4. Perchloric acid: ρ1.67g / mL.

[0030] 1.5. Hydrochloric acid (1+1): The preparation method is to pipette 50mL of the above-mentioned high-grade pure hydrochloric acid into a 100mL beaker with 50mL of water and mix well.

[0031] 1.6. Iron matrix solution (30mg / mL): Weigh 4.285 g of ferric oxide standard into a 250 mL beaker, add 25 mL of hydrochloric acid, cover with a watch glass, heat and dissolve on a hot plate at low temperature, cool, transfer to 100 mL In a volumetric flask, dilute to the mark with water and mix well.

[0032] 1.7, 1000ug / mL standard al...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention belongs to the technical field of industrial analysis, and particularly relates to a method for measuring impurity elements of Al (aluminum), P (phosphor) and Ti (titanium) in nickel concentrate ores. The method comprises the following steps of S1, preparing a sample; S2, preparing a sample solution; S3, preparing a working curve solution; S4, drawing a working curve; S5, measuring the mass concentrations of elements Al, P and Ti in the sample solution; S6, calculating the measuring results, so as to obtain the contents of Al, P and Ti in the sample. The method has the characteristics that the limited number of digestion samples in the microwave digestion process, higher cost of instrument, and high pressure (possibly over-pressure) hidden hazards are overcome, and the defectof difficulty in analysis of industrial large-batch samples is overcome; compared with the atom absorption spectrum instrument and the chemical analysis method, the operation is simple, the analysiscycle is short, the substrate interference-resistant ability is strong, the process is simple, the detection limit is low, the accuracy is good, the precision is high, the to-be-measured elements canbe simultaneously and quickly measured, and the like.

Description

technical field [0001] The invention belongs to the technical field of industrial analysis, in particular to a method for measuring impurity elements aluminum, phosphorus and titanium in nickel concentrate. Background technique [0002] Microwave digestion usually refers to the wet digestion that uses microwaves to heat the digestion solution (various acids, some lyes, and salts) and samples in a closed container to quickly dissolve various samples under high temperature and pressurized conditions. The traditional wet decomposition of samples refers to the method of dissolving various samples through common heating equipment with a certain temperature range. [0003] At present, the determination of multi-elements often uses the ICP-AES method. Impurity elements such as aluminum, calcium, cobalt, chromium, copper, manganese, magnesium, nickel, lead, zinc, etc. in nickel concentrate have been digested by microwave samples and determined by inductively coupled plasma atomic e...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/38G01N21/73
CPCG01N1/38G01N21/73
Inventor 马德莉王学虎
Owner BAIYIN NONFERROUS GROUP
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com