A kind of catalytic cracking catalyst and its preparation method and application
A catalytic cracking and catalyst technology, applied in catalyst activation/preparation, physical/chemical process catalysts, chemical instruments and methods, etc., can solve problems such as large gaps in process conditions, reduce the amount of insoluble matter, reduce the generation of waste residue, reduce The effect of small pollution
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[0053] The preparation method of the catalyst 2-A used in the embodiment of the present invention is as follows: 1) roast the original kaolin powder at 430° C. for 6 h, wherein the heating rate to the roasting temperature is 7° C. / min; 2) step 1) after roasting The obtained kaolin is added to the reactor, and then the impregnating solution of dilute hydrochloric acid of ferric naphthenate and molybdenum naphthenate is added to the reactor for supersaturated impregnation. The amount of the impregnation solution is 1.2 times the theoretical amount of saturated adsorbed water. Ethanol solution, wherein the mass fraction of hydrochloric acid is 12%, stirring during impregnation, the stirring rate is 125r / min, and the stirring time is 1.5h; 3) The material after the reaction in step 2) is dried at 130°C for 4h, and then compressed into tablets Forming, sieving, and taking solid particles with a particle size of 40 mesh to 60 mesh as catalyst 2-A, the added materials meet the followi...
Embodiment 1
[0059]Select a total of 2g of a mixture of 50wt% HDPE, 30wt% PET, and 20wt% PS as the raw material for the reaction of waste plastics, add it to the slurry bed catalytic cracking reactor A, and carry out the process under the catalytic action of the HY molecular sieve catalyst. Catalytic cracking reaction, the addition amount of HY molecular sieve is 12% of the total mass of waste plastics, the reaction conditions of catalytic cracking reaction are as follows: the reaction temperature is 445 ° C, the reaction time is 60 minutes, the stirring speed is 440 rpm, the reaction needs to Pass into hydrogen in the catalytic reactor A, the hydrogen partial pressure is 2.6MPa, the product after reaction is separated, obtains liquid product I, gas I and insoluble matter I; After liquid product I is cooled to room temperature, successively pass into tetrahydrofuran, Hexanaphthene solvent carries out extraction, obtains the tetrahydrofuran solution containing liquid product II, the cyclohex...
Embodiment 2
[0062] Just change the reaction conditions of the catalytic cracking reaction carried out in the catalytic cracking reactor A in the slurry bed catalytic cracking reactor A among the embodiment 1: temperature of reaction is 440 ℃, and the reaction times is 140 minutes, and stirring speed is 480 rev / mins, needs in the reaction Pass hydrogen into the slurry bed catalytic cracking reactor A, the hydrogen partial pressure is 3.4MPa, the conditions for the deep catalytic cracking reaction of the slurry bed catalytic cracking reactor C are changed to: the reaction temperature is 580°C, and the reaction time is 70 minutes , Stirring rate 500 rev / min, need in the reaction feed hydrogen in the slurry bed catalytic cracking reactor C, hydrogen partial pressure is 7.1MPa.
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