Preparation method of graphene and ultrahigh-molecular-weight polyethylene composite fiber
A technology of ultra-high molecular weight and composite fibers, which is applied in the field of preparation of graphene ultra-high molecular weight polyethylene composite fibers, can solve the problems of low surface hardness, difficult molding and processing, and low shear speed, and achieve excellent thermal shock resistance, Effect of improving heat resistance and expanding application range
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Embodiment 1
[0031] The present embodiment provides a kind of preparation method of graphene ultrahigh molecular weight polyethylene composite fiber, specifically comprises the following steps:
[0032] S1: Disperse 100kg of ultra-high molecular weight polyethylene resin and 5kg of silicon carbide in white oil by high-speed shear blending, control the speed of high-speed shear blending at 1500-2800r / min, and form a uniform mixture under heating conditions. resin dispersion;
[0033] S2: adding the graphene dispersion containing 0.5kg graphene powder into the resin dispersion, stirring and heating to obtain a spinning solution;
[0034] S3: The spinning solution is dry-spun at 110° C., and then the raw silk is left to stand and hot-drawn to obtain a graphene ultra-high molecular weight polyethylene composite fiber.
Embodiment 2
[0036] The present embodiment provides a kind of preparation method of graphene ultrahigh molecular weight polyethylene composite fiber, specifically comprises the following steps:
[0037] S1: Disperse 100kg of ultra-high molecular weight polyethylene resin and 20kg of diamond powder in tetralin by high-speed shear blending, control the speed of high-speed shear blending at 1500-2800r / min, and form a uniform resin dispersion;
[0038] S2: adding the graphene dispersion liquid containing 10kg graphene powder into the resin dispersion liquid, stirring and heating to obtain the spinning liquid;
[0039] S3: The spinning solution is dry-spun at 110° C., and then the raw silk is left to stand and hot-drawn to obtain a graphene ultra-high molecular weight polyethylene composite fiber.
Embodiment 3
[0041] The present embodiment provides a kind of preparation method of graphene ultrahigh molecular weight polyethylene composite fiber, specifically comprises the following steps:
[0042] S1: Disperse 100kg of ultra-high molecular weight polyethylene resin and 10kg of ceramic fiber in decahydronaphthalene by high-speed shear blending, control the speed of high-speed shear blending at 1500-2800r / min, and form a homogeneous resin dispersion;
[0043] S2: adding a graphene dispersion containing 5kg of graphene powder into the resin dispersion, stirring and heating to obtain a spinning solution;
[0044] S3: The spinning solution is dry-spun at 110° C., and then the raw silk is left to stand and hot-drawn to obtain a graphene ultra-high molecular weight polyethylene composite fiber.
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