Processing method of easy-to-degrade non-woven fabric with antibacterial function
A processing method and non-woven technology, applied in non-woven fabrics, textiles and papermaking, conjugated rayon, etc., can solve problems such as air pollution, and achieve the effects of strengthening antibacterial properties, good air permeability, and long antibacterial aging.
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Embodiment 1
[0029] (1) Synthesis of carboxyl-terminated polylactic acid: 35g lactic acid is added with water to make lactic acid aqueous solution, and the water pump is decompressed and heated to 160°C for heat preservation and stirring, and the water that is steamed is collected, then 5g adipic acid and 0.1g stannous octoate are added, and the Stir the reaction under reduced pressure with a water pump. After the reaction, the resulting mixture is dissolved in chloroform, precipitated with absolute ethanol, filtered with suction, and then transferred to a vacuum drying oven at 50°C to dry to constant weight to obtain carboxyl-terminated polylactic acid;
[0030] (2) Antibacterial modification of carboxyl-terminated polylactic acid: dissolve 5g of chitosan hydrochloride in water, then add 40g of the prepared carboxyl-terminated polylactic acid, stir fully, and add dilute sulfuric acid dropwise to adjust the pH value to 5, then heat to Heat and stir the reaction in the reflux state. After th...
Embodiment 2
[0035] (1) Synthesis of carboxyl-terminated polylactic acid: 50g lactic acid is added with water to make lactic acid aqueous solution, and the water pump is depressurized and heated to 160°C for heat preservation and stirring, and the water evaporated is collected, then 8g adipic acid and 0.1g stannous octoate are added, and the Stir the reaction under reduced pressure with a water pump. After the reaction, the resulting mixture is dissolved in chloroform, precipitated with absolute ethanol, filtered with suction, and then transferred to a vacuum drying oven at 50°C to dry to constant weight to obtain carboxyl-terminated polylactic acid;
[0036] (2) Antibacterial modification of carboxyl-terminated polylactic acid: dissolve 8g of chitosan hydrochloride in water, then add 50g of the prepared carboxyl-terminated polylactic acid, stir fully, and drop dilute sulfuric acid to adjust the pH value to 5, then heat to Heat and stir the reaction in the reflux state. After the reaction, ...
Embodiment 3
[0041] (1) Synthesis of carboxyl-terminated polylactic acid: 50g lactic acid is added with water to make lactic acid aqueous solution, and the water pump is depressurized and heated to 160°C for heat preservation and stirring, and the water evaporated is collected, then 8g adipic acid and 0.1g stannous octoate are added, and the Stir the reaction under reduced pressure with a water pump. After the reaction, the resulting mixture is dissolved in chloroform, precipitated with absolute ethanol, filtered with suction, and then transferred to a vacuum drying oven at 50°C to dry to constant weight to obtain carboxyl-terminated polylactic acid;
[0042] (2) Antibacterial modification of carboxyl-terminated polylactic acid: dissolve 8g of chitosan hydrochloride in water, then add 50g of the prepared carboxyl-terminated polylactic acid, stir fully, and drop dilute sulfuric acid to adjust the pH value to 5, then heat to Heat and stir the reaction in the reflux state. After the reaction, ...
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