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Extraction method of lilium brownii polysaccharide

A technology of lily polysaccharide and extraction method is applied in the field of plant component extraction to achieve the effect of stable and feasible process conditions

Inactive Publication Date: 2018-06-05
SHANGLUO UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The extraction methods of lily polysaccharides are currently mostly hot water extraction, ultrasonic assisted extraction and enzymatic extraction, etc., among which hot water extraction is the most widely used method, and the water immersion of lily polysaccharides is carried out by using response surface analysis method and orthogonal test method. The optimization of the extraction process is rarely reported

Method used

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  • Extraction method of lilium brownii polysaccharide
  • Extraction method of lilium brownii polysaccharide
  • Extraction method of lilium brownii polysaccharide

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Embodiment Construction

[0017] The technical solution of the present invention will be described in further detail below in conjunction with the accompanying drawings and specific embodiments.

[0018] 1 Materials and methods

[0019] 1.1 Materials

[0020] 1.1.1 Test material

[0021] Lanzhou lily (LiLum davidi) was purchased from Lanzhou City; Shangluo wild lily (Lilium brownii) was collected from Danfeng County.

[0022] 1.1.2 Main reagents

[0023] Phenol, concentrated sulfuric acid, 95% ethanol, glucose, chloroform, and n-butanol were all analytically pure.

[0024] 1.2 Method

[0025] 1.2.1 Test material handling

[0026] Take some fresh lilies, break off the pieces and wash them, dry the water at a constant temperature of 60°C, crush them through a 60-mesh sieve to obtain lily powder, dry and store them for later use.

[0027] 1.2.2 Lily polysaccharide extraction

[0028] Take 2g of lily powder and dissolve it in an appropriate amount of water. After leaching in hot water for a certain...

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Abstract

The invention discloses an extraction method of crotalaria sessiiflora polysaccharide. An optimal technology for extracting lilium brownii polysaccharide, which is optimized through an orthogonal test, is as follows: the extraction time is 2.5h, the temperature is 80 DEG C, the solid-liquid ratio is 1 to 20g / mL and the crude polysaccharide extraction rate is 20.38 percent. A technology for extracting the lilium brownii polysaccharide, which is optimized through a response surface method, is as follows: the extraction temperature is 76 DEG C, the extraction time is 1 hour and 40 minutes, the material-liquid ratio is 1 to 20g / mL and the crude polysaccharide extraction rate is 30.78 percent. The research shows that the response surface method is stably feasible to optimization of technological conditions of a lilium brownii polysaccharide water extraction method, so that theoretical supports are provided for further developing and utilizing Shangluo lily bulbs.

Description

technical field [0001] The invention relates to a method for extracting plant components, in particular to a method for extracting wild lily polysaccharide. Background technique [0002] Lilium (Lilium) is a herbaceous plant of the subclass Liliaceae of monocotyledonous plants. It is named "Lily" because its bulb is composed of many scales. Its bulbs contain a lot of nutrients such as starch, protein, fat, calcium, iron, etc., and some of them can be eaten; its flowers and bulbs are often used as medicinal materials, which have various functions such as clearing the lungs and relieving coughs, soothing the mind, and beautifying the skin. Polysaccharides, alkaloids, saponins and flavonoids are antibacterial active substances in lily, and their medicinal value is anticancer, antiallergic and improving immunity. Lilium brownii (Lilium brownii) mainly grows in the grass on the middle and lower part of the ridge with a steeper slope. Its bulbs are edible and also used as medicin...

Claims

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Application Information

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IPC IPC(8): C08B37/00
CPCC08B37/0003
Inventor 刘长命
Owner SHANGLUO UNIV
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