Preparation method of nanoscale sound insulation glass material

A technology of sound insulation glass and nanomaterials, applied in the field of glass material preparation, can solve problems such as insufficient sound insulation glass, and achieve the effects of improving sound insulation, high sound insulation performance, and excellent sound insulation performance

Active Publication Date: 2018-05-18
安徽强钢钢化玻璃股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The common soundproof glass in the market is divided into hollow glass, vacuum glass and laminated glass. These glasses produce sound insulation eff

Method used

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  • Preparation method of nanoscale sound insulation glass material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] A preparation method of nano-scale sound-insulating glass material, comprising the following steps:

[0016] Step 1. In a warm water bath at 30°C, accurately weigh 4 parts of cetyltrimethylammonium bromide and dissolve it in a mixed solution of 7.8 parts of ethanol and 16.5 parts of deionized water to form a mixture containing cetyltrimethylammonium bromide. A mixture of ammonium bromide;

[0017] Step 2. Add 3 parts of ammonia water with a concentration of 12mol / L to the mixture and stir for 10 minutes, then add 21 parts of Cu-BTC-SiO 2 Nanomaterials and 3 parts of tetraethyl silicate were stirred for 30 minutes, the solution turned into a white suspension, then 2.3 parts of triethyl phosphate was added, stirred for 30 minutes, and then 4.8 parts of calcium nitrate tetrahydrate was accurately weighed and stirred for 1 minute; finally added 5.8 parts of lanthanum nitrate hexahydrate, stirred for 12 hours, filtered with suction, washed 3 times with deionized water and a...

Embodiment 2

[0026] Step 1. In a warm water bath at 30°C, accurately weigh 4 parts of cetyltrimethylammonium bromide and dissolve it in a mixed solution of 7.8 parts of ethanol and 16.5 parts of deionized water to form a mixture containing cetyltrimethylammonium bromide. A mixture of ammonium bromide;

[0027] Step 2. Add 16 parts of ammonia water with a concentration of 12mol / L to the mixture and stir for 10 minutes, then add 28 parts of Cu-BTC-SiO 2 Nanomaterials and 3 parts of tetraethyl silicate were stirred for 30 minutes, the solution turned into a white suspension, then 2.3 parts of triethyl phosphate was added, stirred for 30 minutes, and then 4.8 parts of calcium nitrate tetrahydrate was accurately weighed and stirred for 1 minute; finally added 5.8 parts of lanthanum nitrate hexahydrate, stirred for 12 hours, suction filtered, washed with deionized water and absolute ethanol three times each to obtain a white precipitate; the rest of the preparation was the same as in Example 1. ...

Embodiment 3

[0029] Step 1. In a warm water bath at 30°C, accurately weigh 4 parts of cetyltrimethylammonium bromide and dissolve it in a mixed solution of 7.8 parts of ethanol and 16.5 parts of deionized water to form a mixture containing cetyltrimethylammonium bromide. A mixture of ammonium bromide;

[0030] Step 2. Add 3 parts of ammonia water with a concentration of 12mol / L to the mixture and stir for 10 minutes, then add 35 parts of Cu-BTC-SiO 2 Nanomaterials and 6 parts of tetraethyl silicate were stirred for 30 minutes, the solution turned into a white suspension, then 2.3 parts of triethyl phosphate was added, stirred for 30 minutes, and 4.8 parts of calcium nitrate tetrahydrate was accurately weighed and stirred for 1 minute; finally added 5.8 parts of lanthanum nitrate hexahydrate, stirred for 12 hours, suction filtered, washed with deionized water and absolute ethanol three times each to obtain a white precipitate; the rest of the preparation was the same as in Example 1.

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Abstract

The invention discloses a preparation method of a nanoscale sound insulation glass material. Specifically, a Cu-BTC-SiO2 nanomaterial, ethyl orthosilicate, triethyl phosphate, calcium nitrate terahydrate, lanthanum nitrate hexahydrate and anhydrous sodium carbonate are adopted as the main raw materials, a calcining process is employed to prepare a silica ceramic carrier, the silica ceramic carrieris loaded to a porous organic metal complex Cu-BTC to obtain a high strength Cu-BTC-SiO2 skeleton material, and sound insulation functional particles are evenly distributed in a glass precursor according to the volume complementary filling principle and fuses with glass to form elastic interface bonding, therefore the spatial topological advantages of the metal modified skeleton structure can bebrought into full play. The preparation method provided by the invention is green and environment-friendly, and has little influence on the environment, the obtained product has good sound insulationperformance and wide application range, can be widely applied in the preparation process of various sound insulation glass, and plays an excellent sound insulation role.

Description

technical field [0001] The present invention relates to a method for preparing a nanoscale sound-insulating glass material, which belongs to the field of glass material preparation. Background technique [0002] Sound-insulating glass is a glass product that has a certain shielding effect on sound. It is usually a laminated glass with a multi-layer or multi-layer composite structure. The sound insulation effect can be achieved through the structural design of the glass or the weakening of the sound transmission by the interlayer material. The common soundproof glass in the market is divided into insulating glass, vacuum glass and laminated glass. These glasses produce sound insulation effect from the glass body structure and material level, but in places with high noise requirements, ordinary soundproof glass is far away. not enough. Contents of the invention [0003] The object of the present invention is to provide a nano-scale sound-insulating glass material and a pr...

Claims

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Application Information

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IPC IPC(8): C03C6/00C03C15/00
CPCC03C1/006C03C15/00
Inventor 庄广勇赵方
Owner 安徽强钢钢化玻璃股份有限公司
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