A kind of sintered NdFeB magnet and its preparation method
A technology of NdFeB and magnets, which is applied in the manufacture of inductors/transformers/magnets, magnetic objects, magnetic materials, etc., can solve the problems of development constraints, high prices, and increased production costs of sintered NdFeB magnets, and achieve savings Cost, reduced weight loss, good performance effects
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Embodiment 1
[0018] Example 1: A sintered NdFeB magnet provided in this example is composed of the following components: rare earth element R: 30wt%, Al: 0.8wt%, Pr: 0.04wt%, C: 0.05wt%, Cu : 0.5wt%, Nd: 0.1wt%, Ga: 0.3wt%, Pm: 0.4wt%, Co: 0.9wt%, B: 0.95wt%, Fe balance; the rare earth element R is Ce, Ho, Sm , Dy, Tm mixture, its mixing mass ratio is Ce:Ho:Sm:Dy:Tm=5:4:1:0.3:2.
[0019] The preparation method of the above-mentioned sintered NdFeB magnet comprises the following steps:
[0020] The first step: the mixing of rare earth elements, first remove the rust spots and impurities on the surface of the raw materials of Ce, Ho, Sm, Dy, Tm, and then break them into small pieces with a maximum length, width and thickness of less than 40mm, and then grind them In a powdered state, the mass ratio is Ce: Ho: Sm: Dy: Tm = 5: 4: 1: 0.2: 2. Mix evenly and set aside;
[0021] The second step: batching, remove the surface rust and impurities of the raw material blocks of each component except ...
Embodiment 2
[0030] The preparation method of a sintered NdFeB magnet provided in this example is exactly the same as in Example 1, the main difference is that the mass percentage of the raw material components is different. In this example, the iron-boron magnet is composed of the following components: rare earth Elements R: 28.5wt%, Al: 0.8wt%, Pr: 0.04wt%, C: 0.05wt%, Cu: 0.5wt%, Nd: 0.08wt%, Ga: 0.3wt%, Pm: 0.4wt%, Co : 0.9wt%, B: 0.95wt%, Fe balance; the rare earth element R is a mixture of Ce, Ho, Sm, Dy, Tm, and its mixed mass ratio is Ce: Ho: Sm: Dy: Tm=5 :4:1:0.3:2.
[0031] The obtained product is 20mm×15mm×1.5mm, and its magnetic performance is tested with NIM2000 magnetic measuring instrument of China Metrology Institute. The results are shown in Table 1.
Embodiment 3
[0033]The preparation method of a sintered NdFeB magnet provided in this example is exactly the same as in Example 1, the main difference is that the mass percentage of the raw material components is different. In this example, the iron-boron magnet is composed of the following components: rare earth Elements R: 29.5wt%, Al: 0.8wt%, Pr: 0.04wt%, C: 0.05wt%, Cu: 0.5wt%, Nd: 0.1wt%, Ga: 0.3wt%, Pm: 0.4wt%, Co : 0.9wt%, B: 0.95wt%, Fe balance; the rare earth element R is a mixture of Ce, Ho, Sm, Dy, Tm, and its mixed mass ratio is Ce: Ho: Sm: Dy: Tm=5 :4:1:0.3:2.
[0034] The resulting product is 20mm×15mm×1.5mm, and its magnetic properties are tested with the NIM2000 magnetic measuring instrument of the China Metrology Institute; at the same time, a common NdFeB magnet on the market is 20mm×15mm×1.5mm, and the results are shown in Table 1.
[0035] Table 1:
[0036] Remanence / KGs Magnetic energy product / MGOe Internal coercive force / KOe Example 1 13.23 42....
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