Preparation method of graphene modified high-solid-content high-temperature-resistant epoxy heat-conducting functional coating
A graphene modification and functional coating technology, applied in epoxy resin coatings, anti-corrosion coatings, fire-retardant coatings, etc., can solve the problems of unreachable, large thermal resistance, and insufficient high temperature resistance.
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[0023] 1. Preparation of few-layer graphene dispersion slurry:
[0024] At room temperature, take 150 mg of Grafguard 160-50N by mass, and irradiate with 60 Hz, 900 W microwave for 10 to 60 s under the protection of nitrogen atmosphere to obtain microwave expansion-treated graphite.
[0025] Dissolve an appropriate amount of CTAB in 300 mL of deionized water to prepare an 8.3 mg / mL CTAB aqueous solution.
[0026] Take 50 mg of microwave-expanded graphite and mix it with the above CTAB aqueous solution, place it under ultrasonic conditions, and disperse for 12 to 24 hours to obtain a uniformly dispersed graphene suspension, then filter it with a microporous membrane with a pore size of 0.2 µm, and use it repeatedly. Wash with ion water, filter, centrifuge, dry, finally add AMP-95 amine neutralizer to adjust the pH to 7-9, disperse for 5 minutes, and prepare a few-layer graphene dispersion slurry with a solid content of 5-10% (hereinafter Abbreviated as GSs dispersion slurry). ...
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