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Preparation method of high-chromium vanadium-titanium magnetite pellets

A technology of vanadium-titanium magnetite and vanadium-titanium magnet, which is applied in the field of preparation of high-chromium vanadium-titanium magnetite pellets, which can solve the problems of large fluctuations in the humidity of the mixture, long drying time of the pellets, and long roasting time of the pellets, etc. problems, to achieve the effect of small water loss, shortened drying time, and small water evaporation rate

Inactive Publication Date: 2017-12-15
NORTHEASTERN UNIV LIAONING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] In order to solve the above-mentioned problems of the prior art, the present invention provides a kind of preparation method of high-chromium type vanadium-titanium magnetite pellets, which solves the problems of high water evaporation rate, large water loss and the problem of mixture in the prior art when stewing the material. Humidity fluctuates greatly; pellet drying time is long, pellet surface is not complete; pellet roasting time is long, roasting temperature is high, pellet production efficiency is low, energy consumption is high, and cost is high

Method used

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  • Preparation method of high-chromium vanadium-titanium magnetite pellets

Examples

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Embodiment 1

[0046] A preparation method of high-chromium vanadium-titanium magnetite pellets, reference figure 1 As shown, the method includes:

[0047] 1. Raw material drying

[0048] The high-chromium vanadium-titanium magnetite is dried in a drying box, the drying temperature is 105-108 DEG C, and the drying time is 4 to 4.5h, so that the moisture of the high-chromium-type vanadium-titanium magnetite is less than or equal to 1.4%.

[0049] It has been tested that the moisture content of the high-chromium vanadium-titanium magnetite powder is in the range of 1.2% to 1.4%, which is the crystal water content, and the content exceeding this range is free water; to avoid free water from affecting the dry mixing effect, such as bentonite absorbing high-chromium vanadium The moisture in the titanomagnetite will agglomerate together and reduce the mixing effect with the high-chromium vanadium-titanium magnetite; at the same time, to ensure precise adjustment of the moisture content during the wet mix...

Embodiment 2

[0075] A method for preparing high-chromium vanadium-titanium magnetite pellets. This example is based on Example 1. The specific operation steps are as follows:

[0076] 1. Raw material drying

[0077] Take 5kg of high-chromium vanadium-titanium magnetite and dry it in a drying box. The drying temperature is 108℃ and the drying time is 4h. After drying, the moisture content of the high-chromium-type vanadium-titanium magnetite is 1.2%. .

[0078] 2. Mixing stage

[0079] The calcium-based bentonite is added to the high-chromium-type vanadium-titanium magnetite for dry mixing treatment, and the dry-mixing time is 10 minutes. The calcium-based bentonite added accounts for 0.9% of the weight of the high-chromium-type vanadium-titanium magnetite.

[0080] The high-chromium vanadium-titanium magnetite is then sprayed and wet-mixed, wherein the water is evenly sprayed onto the dry-mixed high-chromium-type vanadium-titanium magnetite through a high-pressure sprayer, and the wet-mixing treatm...

Embodiment 3

[0093] This embodiment is based on embodiment 1, and the specific operations are as follows:

[0094] 1. Raw material drying

[0095] Take 5kg of high-chromium vanadium-titanium magnetite and dry it in a drying box. The drying temperature is 106℃ and the drying time is 4.5h. After drying, the water content of the high-chromium-type vanadium-titanium magnetite is 1.22. %.

[0096] 2. Mixing stage

[0097] The hydrogen-based bentonite is added to the high-chromium-type vanadium-titanium magnetite for dry mixing treatment, and the dry-mixing time is 12 minutes, and the calcium-based bentonite added therein accounts for 1.1% of the weight of the high-chromium-type vanadium-titanium magnetite.

[0098] The high-chromium vanadium-titanium magnetite is then sprayed and wet-mixed, wherein the water is evenly sprayed onto the dry-mixed high-chromium-type vanadium-titanium magnetite through a high-pressure sprayer, and the wet-mixing treatment is performed by spraying water while mixing. The am...

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Abstract

The invention relates to a preparation method of high-chromium vanadium-titanium magnetite pellets. The preparation method comprises the steps that (1) drying high-chromium vanadium-titanium magnetite to enable the moisture content of the high-chromium vanadium-titanium magnetite to be less than or equal to 1.4%; (2) dry-mixing the dried magnetite with bentonite for 10-15 min and then spraying water to conduct wet-mixing for 10-15 min; (3) braising a wet-mixed raw material under the constant-temperature conditions of 25-30 DEG C for 30-35 min; (4) putting the braised raw material into a pelletizer to prepare green pellets with the diameter being 10-12.5 mm; (5) drying the green pellets; (6) sintering the dried green pellets, heating the green pellets to 800-900 DEG C at the heating rate of 10-12 DEG C / min, heating the green pellets to 1150-1200 DEG C at the heating rate of 4-6 DEG C / min and then roasting the green pellets for 15-20 min; and (7) cooling the green pellets to 300 DEG C at the cooling rate of 5-8 DEG C / min and then taking out the pellets for air cooling. By means of the preparation method, the water evaporation rate is small during material braising; the pelletizing efficiency is high; the pellet drying time is short; the compressive strength of dried pellets is high; the roasting temperature is low, and the time is short; the low-temperature reduction degradation rate of the manufactured pellets is high; the reduction expansion rate is small; the reducibility is high; the softening-melting temperature is high; and the softening-melting interval is narrow.

Description

Technical field [0001] The invention belongs to the field of ironmaking raw material production, and specifically relates to a method for preparing high-chromium vanadium-titanium magnetite pellets. Background technique [0002] With the development of vanadium-titanium magnetite smelting technology, the Fe, Ti, V, Cr and other valuable elements in chromium-containing vanadium-titanium ore have been fully utilized, and blast furnace titanium slag, vanadium slag and other resources are comprehensively recycled It provides our country with precious resources of titanium, chromium and vanadium. With the advancement of vanadium-titanium magnetite beneficiation technology, the cost of beneficiation has been reduced, and the output and iron grade have been improved. [0003] The vanadium-titanium magnetite in the Hongge area of ​​Panxi, Sichuan is a complex multi-element associated ore. Its main Fe and Ti elements consist of magnetite, titanomagnetite and ilmenite, and other valuable el...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22B1/24C22B1/02
CPCC22B1/2406C22B1/02C22B1/2413
Inventor 薛向欣汤卫东杨松陶杨合姜涛
Owner NORTHEASTERN UNIV LIAONING
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