Self-etching orthodontic sealing agent and application thereof
A self-etching and sealant technology, which is applied in dental preparations, dental prostheses, and aminohydroxy compound preparations, can solve problems such as the limited effect of fluoride, the lack of good treatment methods for tooth enamel, and the easy side effects of fluoride. , achieve good anti-protein adhesion and antibacterial properties, prevent enamel demineralization, and inhibit the formation of dental plaque
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experiment example 1
[0029] Experimental example 1: Effect of the self-etching orthodontic sealant MSEA of the present invention on the shear bond strength of brackets
[0030] In this experimental example, an experimental study is carried out on isolated premolars to determine whether the self-etching orthodontic sealant MSEA of the present invention will affect the bonding strength of the bracket.
[0031] Specimens: 100 complete premolars extracted due to orthodontics were selected and randomly divided into 5 groups with 20 teeth in each group.
[0032] Choose metal premolar brackets (OPK-A, Tomy, Japan), the area of the bracket floor is 9.94mm 2 .
[0033] grouping:
[0034] 1. Traditional phosphoric acid control group: 37% phosphoric acid (phosphoric acid);
[0035] 2. Self-etching control group: AEO control;
[0036] 3. Anti-protein adhesion group: AEO+7.5%MPC, abbreviation: 7.5%MPC;
[0037] 4. Antibacterial group: AEO+5% DMAHDM, referred to as: 5% DMAHDM;
[0038]5. Mixed group (ie...
experiment example 2
[0045] Experimental Example 2: Effect of the self-etching orthodontic sealant MSEA of the present invention on the long-term stability of the bracket shear bond strength after being used in the oral environment
[0046] Fixed aligners generally need to be worn in the patient's mouth for about 2 years, and the oral environment is very complex, including changes in temperature and humidity, which will affect the bonding strength of the adhesive, resulting in the bracket falling off and affecting the treatment effect. Therefore, an ideal orthodontic adhesive should still have durable bonding strength under the influence of the oral environment, so as to meet clinical requirements. This experimental example simulates the influence of the oral environment on the bonding strength of the bracket through artificial saliva soaking and cold and hot cycle experiments, so as to judge the effect of using the MSEA of the present invention on the long-term stability of the bonding strength of...
experiment example 3
[0060] Experimental example 3: Anti-protein adhesion performance of the self-etching orthodontic sealant MSEA of the present invention
[0061] In this example, the anti-protein ability of the self-etching orthodontic sealant MSEA of the present invention was tested.
[0062] grouping:
[0063] 1. Self-etching control group: AEO control;
[0064] 2. Anti-protein adhesion group: AEO+7.5%MPC, abbreviation: 7.5%MPC;
[0065] 3. Antibacterial group: AEO+5% DMAHDM, referred to as: 5% DMAHDM;
[0066] 4. Mixed group (ie MSEA group): AEO+7.5%MPC+5%DMAHDM.
[0067] Specimen and grouping: Apply the cover of 96-well plate, 1-4 groups are respectively applied to the bottom of the cover groove, pressed with celluloid strips to form a smooth surface, and then cured with visible light for 20 seconds, finally forming a diameter of 8mm, thickness 0.5mm circular test piece. Immerse the test piece in distilled water and stir for 1 h to remove any uncured monomer. All test pieces were drie...
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