Composite silane film for metal surface and preparation method
A technology of composite silane film and metal surface, applied in anti-corrosion coatings, coatings and other directions, can solve problems such as local corrosion and scaling, and achieve the effects of high compactness, simple preparation method and easy large-scale production
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[0030] (1) 304 stainless steel surface chemical pretreatment method
[0031] Cut 304 stainless steel into 1×2cm 2 The rectangular substrate was neutralized with 0.01M HCl solution to remove iron filings on the surface, and treated with 1mol / L NaOH solution for 1 hour to hydroxylate the surface of the stainless steel. Rinse with deionized water and dry for later use.
[0032] (2) Silanization of metal surface
[0033] Add 1,2-bis(triethoxysilyl)ethane to the ethanol-water mixture with a volume ratio of 23:7, so that the volume of 1,2-bis(triethoxysilyl)ethane The percentage is 7%. The 1,2-bis(triethoxysilyl)ethane / ethanol solution should be hydrolyzed for 48 hours before use. Immerse the pretreated 304 stainless steel in the silane solution for 30 minutes, take it out, wash it with isopropanol, absolute ethanol, and acetone to remove excess 1,2-bis(triethoxysilyl)ethane, and dry it at room temperature Then thermal curing treatment was performed at 65° C. for 30 minutes. A...
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