A kind of cathodic electrophoretic paint for leaf spring and preparation method thereof
A technology of cathodic electrophoresis and leaf spring, applied in the field of electrophoretic paint, can solve the problems of low utilization rate, high price, VOC volatilization, etc.
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[0047] In an optional embodiment, the preparation method of the cathodic electrophoretic paint for leaf springs comprises:
[0048] When the epoxy value of the epoxy resin is less than 0.4, put the epoxy resin, epoxy diluent and solvent in the reaction kettle, heat up to 60-100°C, when the epoxy value decreases to 0.07-0.12, continue to add Solvent, when the solution is leveled to a glass state, a toughened epoxy resin is obtained.
[0049] It should be noted that the solvent in the present invention includes: xylene, ethyl acetate, butyl acetate, ethylene glycol monobutyl ether, ethylene glycol monobutyl ether acetate, propylene glycol monomethyl ether, propylene glycol monomethyl ether acetate , propylene glycol monophenyl ether, methyl ethyl ketone, methyl isobutyl ketone or one or more.
[0050] In a preferred embodiment, the solvent is xylene.
[0051] In an optional embodiment, when the epoxy value of the epoxy resin is greater than 0.4, mix the epoxy resin, the chain ...
Embodiment 1
[0075] Put 1600 parts of E-12, 1000 parts of E-20, 1000 parts of polypropylene glycol diglycidyl ether (epoxy value=0.20), 764 parts of polypropylene glycol diglycidyl ether (epoxy value=0.33), and 200 parts of xylene Put it into the reaction kettle, slowly raise the temperature to 100°C, after the material is completely dissolved, add 105 parts of diethanolamine, after reacting at 100°C for 1 hour, add 235 parts of propylene glycol monomethyl ether, 450 parts of ethylene glycol monobutyl ether acetate, Add 141 parts of monoethanolamine, react at 110°C for 2 hours, add 404 parts of polyamide (amine value=320±10mgKOH / g), and react for 2 hours, add 1000 parts of ethylene glycol monobutyl ether, cool to 90°C, add 1600 parts of cross-linking agent, lower the temperature to 70°C, add 2 parts of Tween-40, 2.4 parts of OP-7, 2.4 parts of OP-15, and stir for 1 hour. At 60°C, 117 parts of acetic acid and 176 parts of lactic acid were added and stirred for 0.5 hours. The resin was disc...
Embodiment 2
[0077] Put 1600 parts of E-12, 1000 parts of E-20, 1000 parts of polypropylene glycol diglycidyl ether (epoxy value=0.20), 764 parts of polypropylene glycol diglycidyl ether (epoxy value=0.33), and 200 parts of xylene Put it into the reaction kettle, slowly raise the temperature to 100°C, after the material is completely dissolved, add 105 parts of diethanolamine, and react at 100°C for 1 hour, add 235 parts of propylene glycol monomethyl ether, 450 parts of ethylene glycol monobutyl ether acetate, Add 141 parts of monoethanolamine, react at 110°C for 2 hours, add 404 parts of polyamide (amine value=320±10mgKOH / g), and react for 2 hours, add 1000 parts of ethylene glycol monobutyl ether, cool to 90°C, add 1600 parts of cross-linking agent, lower the temperature to 70°C, add 2 parts of Tween-40, 2.4 parts of OP-7, 2.4 parts of OP-15, and stir for 1 hour. At 60°C, 117 parts of acetic acid and 176 parts of lactic acid were added and stirred for 0.5 hours. The resin was discharge...
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