Method for removing nitrate nitrogen in water, electrode biofilm culturing method, electrode and device
A technology of nitrate nitrogen and film hanging method, applied to electrodes and devices, in the field of removing nitrate nitrogen from water, can solve the problems of weak adsorption force between microorganisms and electrodes, not too high nitrate removal rate, slow film hanging speed, etc. , to achieve the effect of improving the film hanging efficiency, improving the nitrate removal efficiency, and enhancing the utilization rate of the current.
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[0052] The process of magnetization modification of foam nickel electrode comprises the following steps:
[0053] (1) Magnetic Nano Fe 3 o 4 Preparation of:
[0054] 4-6g of Fecl 3 .6H 2 O and 2.78 g of FeCl 2 .7H 2 Dissolve O in 100ml of pure water, then add 2g-3g of polyethylene glycol, stir magnetically, heat to 80-100°C, then add 15ml-20ml of NH 3 .H 2 O, in a nitrogen atmosphere at 60-80°C, react under magnetic stirring conditions for 30-40min, the product is separated by a magnet, washed with pure water, and then vacuum-dried for 6-8h to obtain PEG-Fe 3 o 4 NPS;
[0055] (2) placing the nickel foam after ultrasonic cleaning in a phosphate buffer solution with a concentration of 0.1M and a pH of 7.0 for cyclic voltammetry scanning, and the scanning potential is 0-2.5V;
[0056] (3) 3mg of PEG-Fe 3 o 4 Add NPS into water and ultrasonically disperse for 20-30min to obtain a super-dispersed solution, then apply it on the surface of the activated nickel foam elect...
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