Carrier system for water-soluble active ingredients
An active ingredient and water-soluble technology, which is applied in the field of sunscreen compositions of water-in-silicone inverse emulsions, can solve the problems of long-term stability of light filters such as difficult preparation and lack of stability
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[0064] The preparation methods for each of the examples provided in Tables 1 and 2 were substantially the same. The examples in Tables 1 and 2 include inventive examples of emulsions incorporating high concentrations of water-soluble active ingredients and having water-releasing effects. The examples in Tables 3 and 4 are comparative examples illustrating the lack of emulsion stability and / or stabilization of active ingredients in typical water-in-oil emulsions.
[0065] In each example (inventive example and comparative example), the viscosity of the emulsion was measured using a Brookfield viscometer using a Helipath spindle T-D with a speed set at 10 rpm. The spindle is oscillated in the test sample and the measurement is taken after one minute.
[0066] The water release effect of each example was measured by placing about 0.2 g of the cosmetic composition on the back of the hand and then applying it by gently swirling with the middle and ring fingers of the other hand. ...
Embodiment 13-17
[0087]
[0088]
[0089] In preparing each of the examples in Table 5, the following method was used.
[0090] The components of Phase B (aqueous phase) were mixed together in a side beaker with a rotor / stator stirrer until all solids dissolved, forming a clear solution. If desired, Phase B (aqueous phase) can be heated slowly to about 40-45°C until all solids are dissolved. The ingredients of phase A (oil phase) were placed in the main beaker and mixed well with a propeller stirrer at about 600-700 RPM, then set aside. Slowly add the mixture of water phase (Phase B) ingredients to the combined Phase A (oil phase) ingredients and mix using a propeller mixer for 10-15 minutes for batches of about 1 kg. As the viscosity of the mixture increased, the stirring rate was increased from 700 rpm to about 1200 rpm. As the water phase is mixed into the oil phase, a water-in-oil emulsion forms. Optionally, powder is added to the batch and mixed into the water-in-oil emulsion.
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