Rare-earth-cobalt-based composite material
A composite material and composite magnetic material technology are applied in the field of rare earth cobalt-based composite materials to achieve the effects of saving raw material costs, reducing raw material costs and improving coercivity.
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preparation Embodiment 1
[0056] The preparation method of this embodiment includes the following steps: 1), smelting and casting the raw materials of the matrix to obtain ingots; 2), hydrogen breaking; 3), jet milling; 4), magnetic powder mixing; 5), orientation molding, Cold isostatic pressing and heat treatment to obtain rare earth cobalt-based composite materials; the heat treatment is to heat the blank obtained by cold isostatic pressing to 1100°C for 4.5 hours, and then lower it to 930°C at a cooling rate of 0.4°C / min for 13 hours and keep it in the air. Cool to room temperature, then keep warm at 760°C for 5 hours, then slowly cool to 360°C at a cooling rate of 0.8°C / min and keep warm for 3 hours, then air-cool to room temperature.
preparation Embodiment 2
[0058] The preparation method of this embodiment includes the following steps: 1), smelting and casting the raw materials of the matrix to obtain ingots; 2), hydrogen breaking; 3), jet milling; 4), magnetic powder mixing; 5), orientation molding, Rare earth cobalt-based composite materials are obtained by cold isostatic pressing and heat treatment; the heat treatment is to heat the blank obtained by cold isostatic pressing to 1150°C for 5.5 hours, and then lower it to 950°C at a cooling rate of 4°C / min for 5 hours and keep it in the air. Cool to room temperature, then keep warm at 820°C for 40 hours, then slowly cool to 500°C at a cooling rate of 2.4°C / min and keep warm for 2 hours, then air-cool to room temperature.
preparation Embodiment 3
[0060] The preparation method of this embodiment includes the following steps: 1), smelting and casting the raw materials of the matrix to obtain ingots; 2), hydrogen breaking; 3), jet milling; 4), magnetic powder mixing; 5), orientation molding, Cold isostatic pressing and heat treatment to obtain rare earth cobalt-based composite materials; the heat treatment is to raise the temperature of the blank obtained by cold isostatic pressing to 1200°C for 3.5 hours, and then reduce it to 1050°C at a cooling rate of 3°C / min for 15 hours and keep it in the air. Cool to room temperature, then keep warm at 780°C for 20 hours, then slowly cool to 400°C at a cooling rate of 3.1°C / min and keep warm for 1 hour, then air cool to room temperature.
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